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u3@2 o2 laboratories <br /> iGround Zero Analysis <br /> 1714 Main Street Date(s)Sampled 05/28/03 <br /> Escalon,CA 95320 05130/03 <br /> Date Received 05/30103 <br /> Prot ID 186 Volatile Organics By GC/MS Date Analyzed 06/03/03 <br /> Site Knowles Roek <br /> Method EPA 8260B <br /> Lab ID D05489(d) D05490 D05491 D05492 <br /> Sample ID KR MW14 KR MW15A KR MW158 KR MW15C <br /> Matrix Water Water Water Water <br /> t-Butanol(TBA) <10,000 <20 <20 <20 <br /> Methyl-t-Butyl Ether(MTBE) 100,000 33 190 <2 0 <br /> DI-Isopropyl Ether(DIPE) <1,000 <20 <2 0 <2 0 <br /> Ethyl-t-Butyl Ether(ETRE) <1,000 <2 0 <2 0 <2 0 <br /> t-Amyl Methyl Ether(TAME) <1,000 <2 0 <2 0 <20 <br /> 1,2-Dlchloraethane(1,2-DCA) <1,000 47 90 <2 0 <br /> 1,2-Dibromoethane(EDB) <1,000 <20 <2 0 <2 0 <br /> QAIQC <br /> Surrogate Spike Recovery 101% 89% 98% 100% <br /> (d) Sample diluted due to high ooncentration of target analytes and/or high organic content <br /> Note Water samples are reported inµglL,sod and sludge samples in mglKg <br /> Hiramueto <br /> Lab Director <br /> DHS Cerhficatlon No 2359 <br /> i <br /> 3037 Fifth St, Ceres, CA 95307 • Phone (209)581-9280 • Fax (209) 581-9282 <br />