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r <br /> 110 Second Avenue South #D7,Pacheco,CA 94553 <br /> r McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> htt //www mccam bell com E-mail main@mccampbell cam <br /> Remedy, Inc Client Protect ID Frank's One Stop Date Sampled 06/05/98 <br /> r 112 Dove Court Date Received 06/05/98 <br /> Vacaville,CA 95687 Client Contact Paul LeCheminant Date Extracted 06/11/98 <br /> rClient P O Date Analyzed 06111-06112/98 <br /> Volatile Organics By GC/MS <br /> EPA method 8260 <br /> r Lab ID 90153 <br /> Client ID Franks TR-3 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone ND<100 Ethylbenzene 140 <br /> Benzene ND<20 HeraLhlorobutadiene ND<20 <br /> Bromobenzene NIK20 lodomLthane ND<20 <br /> Bromochloromethane ND<20 lsopropylbLnzene 33 <br /> Bromodichloromethane ND<20 p-Isopropyl toluene ND<20 <br /> Bromoform ND<20 Methyl butyl ketone ' ND<20 <br />' Bromomethane ND<20 Methylene Chloride" ND<20 <br /> n-Butyl benzene 97 Methyl ethyl ketone ND<20 <br /> sec-Butyl benzene ND<20 Methyl isobutyl ketones ND<20 <br /> tert-Butyl benzene 96 Methyl tert-Butyl Ether(MTBE) ..- <br /> Carbon Disulfide ND<20 Naphthalene 46 <br /> Carbon Tetrachloride ND<20 n-Propyl benzene 260 <br /> Chlorobenzene ND<20 Styrene` ' ND<20 <br /> Chloroethane ND<20 1 1,1 2-Tetras.h loroethane ND<20 <br /> 2-Chloroethyl Vinyl Ether"' ND<20 1 1 2 2-Tetrachloroethane ND<20 <br /> Chloroform ND<20 Tetrachlorocthene ND<20 <br /> Chloromethane ND<20 Toluene... ND<20 <br /> 2-Chlorotoluene ND<20 1 2 3-1 rich Iorobenzene ND<20 <br /> 4-Chlorotoluene ND<20 l 2 4-Trichlorobenzene ND<20 <br /> Dibromochloromethane ND<20 1,1 1-Trichloroethane ND<20 <br /> 12-Dibromo-3-chloropropane ND<20 1,12-trichloroethane ND<20 <br /> Dibromomethane ND<20 Trichloroethene ND<20 <br /> 12-Dichlorobenzene ND<20 Trichlorotluoromethane ND<20 <br /> 1,3-Dichlorobenzene ND<20 1 2 3-Trichloropropane ND<20 <br /> 14-Dichlorobenzene ND<20 1 2 4-Trimethylbenzene ND<20 <br /> Dtchlorodifluoromethane ND<20 1,3 5-Tnmethylbenzene 260 <br /> I 1,1-Dichloroethane ND<20 Vinyl Acetate""' NIK20 <br /> 12-Dichloroethane ND<20 Vinyl Chloride " ND<20 <br /> I I-Dichloroethene ND<20 Xylenes total '°' 1300 <br /> cis-[ 2-Dichloroethene ND<20 <br /> trans-1,2-Dichloroethene ND<20 <br /> 12-Dichloropropane ND<20 <br /> l 3-Diichloropropane ND<20 <br /> 2 2-Dichloropropane ND<20 Comments <br /> I I-Dichloropropane ND<20 Surrogate Recoveries <br /> cis-13-Dichloropropane ND<20 Dibromolluoromethane Ill <br /> trans-l,3-Dichloropropene ND<20 Toluene-d8 95 <br /> Ethylene dibromide ND<20 4-Bromotluorobenzene 94 <br /> Iwater and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples I ug/L,vapor samples 0 5 ug/L,solid and sludge samples 5 ug/kg wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone, (c) (2-chloroethoxy) ethene (d) 2-hexanone (c) dichloromethane (t) 2-butanone (g) 4-methyl-2 <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present (i) liquid sample that contains greater than --5 vol % <br /> sediment,(1)sample diluted due to high organic content, (k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte (1)methylbenzene,(m)acetic acid ethenyl ester (n)chloroelhene (o)dimethylbenzenes <br /> DHS Certification No 1644 / Edward Hamilton, Lab Director <br />