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110 Second Avenue South,#D7,Pacheco,CA 94553 <br /> 4 MCCAWBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> http/lwww mccampbell com E-mail main@mccampbell com <br /> Remedy, Inc Client Project ID Frank's One Stop Date Sampled 06/10/98 <br /> 112 Dove Court Date Received 06/10/98 <br /> Vacaville, CA 95687 Client Contact Paul LeCheminant Date Extracted 06/I0/98 <br /> Client P O Date Analyzed 06110-06/11/98 <br /> Volatile Organics By CC/MS <br /> EPA method 8260 <br /> Lab ID 90305 <br /> Client ID Franks TR-9A <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> Acetone' ' ND<2500 Ethylbenzene 440 <br /> Benzene ND<250 Hexachlorobutadiene ND<250 <br /> Bromobenzene ND<250 lodomethane ND<250 <br /> Bromochloromethane ND<250 lsapropylbenzt ne ND<250 <br /> Bromodichloromethane ND<250 p-Isopropyl toluene ND<250 <br /> Bromoform ND<250 Methyl butyl ketone' ' ND<250 <br /> Bromomethane ND<250 Methylene Chloride" ND<250 <br /> n-Butyl benzene ND<250 Methyl ethyl ketone ND<250 <br /> sec-Butyl benzene ND<250 Methyl isobutyl ketones ND<250 <br /> tert-Butyl benzene ND<250 Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND<250 Naphthalene ND<250 <br /> Carbon Tetrachloride ND<250 n-Propvl benzene 300 <br /> Chlorobenzene ND<250 Styrene' ND<250 <br /> Chloroethane ND<250 1,1,1 2-Tetrachloroethane ND<250 <br />' 2-Chloroethyl Vinyl Ether"' ND<250 1,1 2 2 TetrachlorMthane N13<250 <br /> Chlorotorrn ND<250 Tetrachlorat.[Ilene ND<250 <br /> Chloromethane ND<250 Toluene" 680 <br /> 2-Chlorotoluene ND<250 1 2 3-Truhlorobenzene ND<250 <br /> 4-Chlorotoluene ND<250 1 2 4-Tnchlorobenzene ND<250 <br /> Dibromochloromethane ND<250 1,l I-Trichloroethane ND<250 <br /> 12-Dibromo-3-chloropropane ND<250 I 12-Tnehloroethane ND<250 <br /> Dibromomethane ND<250 Trichloroethene ND<250 <br /> 1,2-Dichlorobenzene ND<250 Trichloroiluoromethane NDc250 <br /> 1 3-Dichlorobenzene ND<250 1,2 3-Trichloropropane ND<250 <br /> 14-Dichlorobenzene ND<250 1,2 4-Trimethylbenzene 1100 <br /> Dichlorodifluoromethane ND<250 1 3 5-Tnmethylbcnzene 300 <br /> 1.1-Dichloroethane ND<250 Vinyl Acetate "' ND<250 <br /> 1,2-Dichloroethane ND<250 Vinyl Chloride " ND<250 <br /> l,1-Dichloroethene ND<250 Xylenes total 3500 <br /> cis-1,2-Dichloroethene ND<250 <br /> trans-1,2-Dichloroethene ND<250 <br /> l,2-Dichloropropane ND<250 <br /> 13-Dichloropropane ND<250 <br /> 2 2-Dtchloropropane ND<250 Comments <br /> I I-Dichlororopene ND<250 Surrogate Recoveries <br /> cis-1,3-Dichloropropene ND<250 Dibromotluoromethane 107 <br /> trans-13-Dichloropropene ND<250 Toluene-d8 94 <br /> Ethylene dibromide ND<250 4-Bromotluorobenzene 89 <br /> water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated water samples 1 ug/L,vapor samples 0 Sug/L,solid and sludge samples 5 ug/kg wipes 0 2ug/wipe <br /> ND means not detected above the reporting limit,N/A means analyte not applicable to this analysts <br /> (b) 2-propanone or damethyl ketone, (c) (2-chloroethoxy)ethene (d) 2-hexanone (e)dichloromethane (1) 2-butanone (g) 4-methyl-2- <br /> pentanone or isopropylacetone, (h) lighter than water immiscible sheen is present, (i) liquid sample that contains greater than —5 vol % <br /> sediment 0)sample diluted due to high organic content, (k)peaks present in this carbon range do not match the pattern of our standard fo <br /> this analyte (1)methylbenzene;(m)acetic acid ethenyl ester (n)chloroethene (o)dimethylbenzenes <br /> DHS Certification No 1644 Edward Hamilton, Lab Director <br />