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I I( Second Avenue South,##1)7,Pacheco,CA 94553 <br /> MCCAMPBELL ANALYTICAL INC. cleplzone : 510-798-1620 Fax : 510-798-1622 <br /> hap lhv vw.mccam pbcll.com E-mail:main@mccampboll.com <br /> Client Pro ect ID: 5-Starr Manna Date S impled: 11/18/97 <br /> Advanced GeoEnviroaimental 3 <br /> Date Received: 11/20/97 <br /> 4005 North Wilson Way <br /> Stockton, CA 95205 Client Contact: Bill Little Date Extracted: 11/20/97 <br /> Client P-O: Date Analyzed: 11/20-11124/97 <br /> Volatile Organics ByGUMS <br /> EPA method 8260 <br /> Lab ID 83234 <br /> Client ID SP1-1 <br /> Matrix S <br /> Compound Concentration* i i <br /> Compound Concentration* <br /> Acetone ND<7 Ethylbenzene ND <br /> Benzene ND Hexachlorobutadiene ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND Isopropylbenzene ND <br /> Bromodichloromethane ND p-Isopropyl toluet e ND <br /> Bromoform ND Methyl butyl ket ne' ' ND <br /> Bromomethane ND Methylene Chlori e'er' ND <br /> n-Butyl benzene ND Methyl ethyl ketotcND <br /> sec-Butyl benzene ND Methyl isobutyl k tone's ND <br /> tert-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) --- <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene NO Styrene' ' ND <br /> Chloroethane ND 1,1,1,2-Tetrachio oethane ND <br /> 2-Chloroethyl Vinyl Ether` ND 1,1,2,2-Tetrachloi oethane ND <br /> Chloroform ND Tetrachloroethend ND <br /> Chloromethane ND Toluene" ND <br /> 2-Chlorotoluene ND 1,2,3-Trichlorobe zene ND <br /> 4-Chlorotoluene ND 1,2,4-Trichlorobe azene ND <br /> Dibromochloromethane ND 1,1,1-Trichloroet ane ND <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Trichloroetl iane ND <br /> Dibromomethane ND Trichloroethene ND <br /> 1,2-Dichlorobenzene ND Trichlorofluoront thane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Trichloropr pane ND <br /> l,4-Dichlorobenzene ND 1,2,4-Trimethylb nzene ND <br /> Dichlorodifluoromethane ND 1,3,5-Trimethylb nzene ND <br /> M-Dichloroethane ND Vinyl Acetate""' ND <br /> 1,2-Dichloroethane ND Vinyl Chloride"" ND <br /> l,l-Dichloroethene ND Xylenes,total '°' ND <br /> cis-1,2-Dichloroethene ND TPH-(g)(CO-C 12) --- <br /> trans-1,2-Di chloroethene ND TPH-(ms)(C8-G12) --- <br /> 1,2-Dichloropropane ND TPH-(k)(C10+) --- <br /> 1,3-Diehl oropropane ND <br /> 2,2-Dichloropropane ND Comments: <br /> 1,1-Dichloropropene ND Surrogate Recoveries(`%o) <br /> cis-1,3-Dichloropropene ND Dibrosnotluorom thane 108 <br /> trans-1,3-Dichloropropene ND Toluene-d8 107 <br /> Ethylene dibromide ND 4-Bromoduorobe zene 97 <br /> "water and vapor samples are reported in ug/L,soil and sludge samples in ug/k .wipes in ug/wipe and all TCLP I SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 0.5 ug/L; vapor s mples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;N/A means analyte not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hex none; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2- <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is pr sent; (i) liquid sample that contains greater than --5 vol. % <br /> sediment;0?sample diluted due to high organic content;(k)peaks present in 11fis carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester,(n)chloroethene;(o)dimethylbenzenes. <br /> DHS Certification No. 1644 LEdward Hamilton,Lab Director <br />