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<br /> I I G Second Avenue S(Rdh,9137, Pacheco,CA 94553
<br /> McCAMPBELL ANALYTICAL INC. IIelcphonc :510-798-1620 Fax :510-795-1622
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<br /> Advanced GeaEnvironmental J
<br /> Client Project ID: 5-Starr Mat ina nate Sampled: 11/18/97
<br /> 4005 North Wilson Way Date Received: 11/20/97
<br /> Stockton,CA 95205 Client Contact:Bill Little Date Extracted: 11/20/97
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<br /> Client P.O: Date Analyzed: 11120-11/24197
<br /> Volatile Organics By GC/MS
<br /> EPA method 8260
<br /> Lab ID 83236
<br /> Client ID TI-E
<br /> Matrix S
<br /> Compound Concentration* Compound Concentration*
<br /> Acetone" ND Ethylbenzene ND
<br /> Benzene ND Hexachlorobutad ene ND
<br /> Bromobenzene ND lodomethane ND i
<br /> Bromochloromethane ND lsopropylberizent ND
<br /> Bromodichloromethane ND p-Isopropyl t011le le ND
<br /> Bromoform ND Methyl butyl ketone` ' ND
<br /> Bromomethane ND Methylene Chlor de" ND<6
<br /> n-Butyl benzene ND Methyl ethyl ketc ne" ND
<br /> sec-Butyi benzene ND Methyl isobutyl ketone'S ND
<br /> tent-Butyl benzene ND Methyl tert-Butyl Ether(MTBE) —
<br /> Carbon Disuitide ND Napthalene 8.3
<br /> Carbon Tetrachloride ND n-Propyl benzene ND
<br /> Chlorobenzene ND Styrene`' ND
<br /> Chloroethane ND 1,1,1,2-Tetrachlo oethane ND
<br /> 2-Chloroethyl Vinyl Ether" ND 1,1,2,2-Tetrachlo oethane ND
<br /> Chloroform ND Tetrachloroethene ND<8
<br /> Chloromethane ND Toluene" ND
<br /> 2-Chiorotoluene ND 1,2,3-Trichlorob nzene ND
<br /> 4-Chiorotoluene ND 1,2,4-Trichlorob nzene ND
<br /> Dibromochloromethane ND 1,1,1-Trichloroetiane ND
<br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Trichloroetiane ND
<br /> Dibromomethane ND Trichloroethene ND
<br /> 1,2-dichlorobenzene ND Trichlorotlumo ethane ND
<br /> 1,3-Dichlorobenzene ND 1,2,3-Tricltlorop pane ND
<br /> 1,4-Dichlorobenzene ND 1,2,4-Trimethylb nzene 1 i
<br /> Dichlorodifluoromethane ND 1,3,5-Trimethylb nzene ND
<br /> l,l-Dichloroethane ND Vinyl Acetate""' ND
<br /> 1,2-Dichloroethane ND Vinyl Chloride"' ND
<br /> l,l-Dichloroethene ND Xylenes,total '° 17
<br /> cis-1,2-Dichloroethene ND TPH-(g)(C6-C11 2) -
<br /> trans-l,2-Dichloroethene ND TPH-(ms)(C8-1.12) ---
<br /> 1,2-Dichloropropane ND TPH-(k)(C10}) ---
<br /> 1,3-Dichloropropane ND
<br /> 2,2-Dichloropropane ND Comments:
<br /> 1,1-Dichloropropene ND Surrogate Recoveries(%)
<br /> cis-1,3-Dichloropropene ND Dibromotluorom thane 113
<br /> trans-l,3-Dichloropropene ND Toluene-d8 108
<br /> Ethylene dibromide ND 4-Bromotluorob nzene 103
<br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/k,,,,wipes in ug/wipe and all TCLP I SPLP extracts in ugJL
<br /> Reporting limits unless otherwise stated: water samples 0.5 Lig/L; Vapor s mples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes
<br /> 0.2ug/wipe ND means not detected above the reporting limit;NIA means anal to not applicable to this analysis
<br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hes none; (e) dichloromethane; (f) 2-butanone; (g) 4-methyl-2-
<br /> pentanone or isopropy[acetone; (h)lighter than water immiscible sheen is p esent, (i) liquid sample that contains greater than —5 vol. %
<br /> sediment;0)sample diluted due to high organic content;(k)peaks present in his carbon range do not match the pattern of our standard for
<br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;(o)dimethyibenzenes.
<br /> DHS Certification No. 1644 Edward Hamilton,Lab Director
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