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I 10 Second AveHue Soolh,#fD7,Pacheco,CA 94553 <br /> McCAMPBELL ANALYTICAL INC. Telephonc : 510-798-1620 Fax : 510-798-1622 <br /> http://w vw.ntccam 7bcll.coHi E-mail:main@mccantpbeli.com <br /> Dat <br /> Advanced GeoEnvironmental Client Project ID: 5-Starr Marina e Sampled: 11/18/97 <br /> I <br /> 4005 North Wilson Way <br /> Date Received: 11/20/97 <br /> Stockton, CA 95205 Client Contact: Bill Little Date Extracted: 11/20/97 <br /> i <br /> Client P.O: Date Analyzed: 11/20-11/24/97 <br /> Volatile Organics ByGC/MS <br /> PA method 8260 <br /> Lab ID 83235 <br /> Client ID SP2-1,2 <br /> Matrix S <br /> Compound Concentration* Compound Concentration* <br /> AcetoneND<7 Ethylbenzene ND I <br /> Benzene ND Hexachlorobutadi ne ND <br /> Bromobenzene ND lodomethane ND <br /> Bromochloromethane ND lsopropylbenzeoe ND <br /> Bromodichloromethane ND p-Isopropyl toluene ND I� <br /> Bromoform ND Methyl butyl ketor e` ' ND <br /> Bromomethane ND Methylene Chloric e" ND <br /> Ti-Butyl benzene ND Methyl ethyl ketole" ND <br /> sec-Butyl benzene ND Methyl isobutyl kt tone`s ND <br /> tert-Butyl benzene ND Methyl tert-Butyl ther(MTBE) - <br /> Carbon Disulfide ND Napthalene ND <br /> Carbon Tetrachloride ND n-Propyl benzene ND <br /> Chlorobenzene ND Styrene LU AID <br /> Chloroethane ND 1,1,1,2-Tetrachlor ethane ND <br /> 2-Chloroethyl Vinyl Ether` ND 1,1,2,2-Tetrachlor ethane ND <br /> Chloroform ND Tetrachloroethene ND <br /> Chloromethane ND Toluene" ND <br /> 2-Chlorotoluene ND 1,23-Trichiorobei zene ND <br /> 4-Chlorotoluene ND 1,2,4-Tricblorober zene ND i <br /> Dibromochloromethane ND 1,1,1-Trichloroeth me ND , <br /> 1,2-Dibromo-3-chloropropane ND 1,1,2-Trichloroeth ne ND i <br /> Dibromomethane ND Trichloroethene ND <br /> i <br /> 1,2-Dichlorobenzene ND TrichlOrOflnorome hane ND <br /> 1,3-Dichlorobenzene ND 1,2,3-Trichloropro ane ND <br /> 1,4-Dichlorobenzene ND 1,2,4-Trimethylbei zene ND <br /> Dichlorodifluoromethane ND 1,3,5-Trimethylbe zene ND <br /> 1,1-Dichloroethane ND Vinyl Acetate""' ND <br /> 1,2-Dichloroethane ND Vinyl Chloride"" ND <br /> l,l-Dichloroethene ND Xylenes,total '°' ND <br /> cis-1,2-Dichloroethene ND TPH-(g)(C6-C l ) -- <br /> trans-l,2-Dichloroethene ND TPH-(ms)(CS-C 2) -- <br /> 1,2-Dichloropropane ND TPH-(k)(C 10+) --- <br /> 1,3-Dichloropropane ND <br /> 2,2-Dichloropropane ND Comments; <br /> IJ-Dichloropropene ND Surrogate Recoveries("/„) <br /> cis-1,3-Dichloropropene ND Dibromotluorome Kane 107 <br /> trans-1,3-Dichloropropene ND Toluene-0 109 <br /> Ethylene dibromide ND 4-Brom0tluorobenzene 100 i <br /> 'water and vapor samples are reported in ug/L,soil and sludge samples in ug/kg,wipes in ug/wipe and all TCLP/SPLP extracts in ug/L <br /> Reporting limits unless otherwise stated: water samples 0.5 ug/L; vapor sarnples 0.5 ug/L; solid and sludge samples 5 ug/kg; wipes <br /> 0.2ug/wipe ND means not detected above the reporting limit;N/A means analyze not applicable to this analysis <br /> (b) 2-propanone or dimethyl ketone; (c) (2-chloroethoxy) ethene; (d) 2-hexa one; (e) dichloromethane; (t) 2-butanone; (g) 4-methy9-2- <br /> pentanone or isopropylacetone; (h) lighter than water immiscible sheen is pre ent; (i) liquid sample that contains greater than—5 vol. % <br /> sediment;0)sample diluted due to high organic content;(k)peaks present in this carbon range do not match the pattern of our standard for <br /> this analyte;(1)methylbenzene;(m)acetic acid ethenyl ester;(n)chloroethene;( )dimethylbenzenes. <br /> DHS Certification No. 1644 / Edward Hamilton,Lab Director <br />