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Enviro-Chem, Inc. <br />1214 E. Lexington Avenue, Pomona, CA 91766 Tel (909)590-5905 <br />8270C QA/QC Report <br />Matrix: Soil/Solid/Sludge/Oil <br />Date Analyzed: 8/17/2018 <br />Matrix Spike (MS)/Matrix Spike Duplicate (MSD) <br />Spiked Sample Lab I.D.: 180813-103 MS/MSD <br />Fax (909)590-5907 <br />unit: nigNi (PPM) <br />Analyte <br />SR <br />s k conc <br />MS <br />%MS j <br />MSD <br />%MSD <br />%RPO ACP %MSI <br />ACP RPD <br />Phenol <br />0.0 <br />2.00 <br />1.59 <br />80% 1 <br />1.33 <br />67% <br />_ 18% 1 50-150 1 <br />0-20 <br />Pyrene <br />0.0 <br />2.00 <br />1.79 <br />90% <br />2.09 <br />104% <br />1 15% 1 50-150 1 <br />0-20 <br />Laboratory Control Spike (LCS): <br />Analyte s k conc <br />Phenol 2.00 <br />1,4 -Dichlorobenzene 2.00 <br />2,4-Dichlorophenol 2.00 <br />Hexachlorobutadiene 2.00 <br />4 -Chloro -3 -meth I hence 2.00 <br />Fluoranthene 2.00 <br />LCS <br />1.88 <br />1.94 <br />1.90 <br />1.96 <br />1.82 <br />2.04 <br />% RC <br />94% <br />97% <br />95% <br />98% <br />91% <br />102% <br />ACP °ioRc <br />75-125 <br />75-125 <br />75-125 <br />75-125 <br />75-125 <br />75-125 <br />Surrogate Recovery <br />s k conc <br />ACP% <br />%RC <br />I %RC <br />%RC <br />°SRC <br />%RC %RC <br />%RC <br />Sam le I.D. <br />MB <br />1180813-1031180813-1051180813-106]180813-16.71180815-151 <br />180815-19 <br />2-Fluorophenol <br />40 <br />25-121 <br />114% <br />1 123*% <br />129*% <br />127`% <br />124*% 122"% <br />133*% <br />Phenol -d5 <br />40 <br />24-113 <br />98% <br />111% <br />117*% <br />115 % <br />110% 107% <br />118*% <br />Nitrobenzene -d5 <br />40 <br />23-120 <br />107% <br />122*% <br />126"% <br />124*% <br />121 *% 119% <br />130*% <br />2-Fluorobiphen I <br />40 <br />30-115 <br />101% <br />138*% <br />140*% <br />140*% <br />136*% 132`% 1 <br />145*% <br />2,4,6-Tribromo henol <br />40 <br />19-122 <br />70% <br />104% 1 <br />105% 1 <br />97% <br />93% 93% <br />L 91% <br />Ter hen I -d14 <br />1 40 <br />18-137 <br />118% <br />1 213*% <br />224*% <br />247*% <br />244*% 213*% <br />253*% <br />.Surrogate Recove <br />spk conc <br />ACP% <br />%RC <br />I °IRC <br />"1 RC <br />%RC <br />%RC %RC I <br />RG <br />Sample I. D. <br />180815-1 <br />180807-13 <br />180816-31 <br />2-Fluorophenol <br />40 <br />25-121 <br />147*% <br />105% <br />105% <br />Phenol -d5 <br />40 <br />24-113 <br />138*% <br />96% <br />91% <br />_ <br />Nitrobenzene -d5 <br />40 <br />23-120 <br />145*% <br />103% <br />98% <br />2-Fluorobiphenyl <br />40 <br />30-115 <br />143*% <br />101% <br />97% <br />2,4,6-Tribromo henol <br />40 <br />19-122 <br />175*0/( <br />880X <br />76% <br />Terphenyl-d14 <br />40 <br />18-137 <br />192*% <br />134% <br />126% <br />Surrogate Recovery I <br />spk conc <br />ACP% <br />%RC <br />%FSC <br />%RC <br />%RC <br />%RC %RC <br />%RC <br />Sample I.D. <br />2-Fluorophenol <br />40 <br />25-121 <br />Phenol -d5 <br />44 <br />24-113 <br />Nitrobenzene -d5 <br />40 <br />23-120 <br />2-Fluorobiphen I <br />40 <br />30-115 <br />2,4,6-Tribromo henol <br />40 <br />19-122 <br />Terphenyl-d14 <br />40 <br />18-137 <br />* = Surrogate fail due to matrix interference <br />Analyzed and Reviewed By; (—f Mote; LCS, MS, MSD are in control therefore results are in control. <br />Final Reviewer: <br />