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110 2nd Avenue South,4D7,Pacheco,CA 94553-5560 <br /> McCAMPBELL ANALYTICAL INC Telephone 925-798-1620 Fax 925-798-1622 <br /> ' httn//www mccampbell com E-mail main@mccampbell com <br /> i <br /> Advanced GeoEnvironmental Client Project ID Five Starr Marina Date Sampled 08/03/99 <br /> 4005 North Wilson Way Date Received 08/04/99 <br /> Stockton, CA 95205 Client Contact Bill Little Date Extracted 08/05-08/06/99 <br /> Client P O Date Analyzed 08/05-08/06/99 <br /> Oxygenated Volatile Organics By GC/MS <br /> EPA method 8260 modified <br /> Lab ID 16618 16619 16620 16621 <br /> Reporting Limit <br /> Client 1D MW-1 MW-3 MW4 MW-5 <br /> Matrix W W W W S W <br /> Compound Concentration* ug/kg ug/L <br /> Di-isopropyl Ether(D1PE) ND<1 5 ND ND ND 50 1 0 <br /> Ethyl tent-Butyl Ether(ETBE) ND<l 5 ND 27 ND so 1 0 <br /> Methyl-tert Buty]Ether(MTBE) ND<l 5 ND 64 ND 5 0 1 0 <br /> tert-Amyl Methyl Ether(TAME) ND<1 5 ND ND ND 50 1 0 <br /> tert-Butanol ND<8 ND ND ND 25 5 0 <br /> Surrogate Recoi eries(%) <br /> Dibromofluoromethane 95 96 103 104 <br /> Comments J <br /> *water samples are reported in ug/L,soil and sludge samples in ug/kg Hipes in ug/wipe and all TCLP I STLC I SPLP extracts in ug/L <br /> ND means not detected above the reporting limit NIA means surrogate not applicable to this analysis <br /> (h)lighter than Mater immiscible sheen is present,(i)liquid sample that coniainw greater than—5 vol %sediment,0)sample diluted due to <br /> high organic content <br /> DHS Certification No 1644 Edward Hamilton,Lab Director <br />