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110 2nd Avenue South,#D7,Pacheco,CA 94553 <br /> McCAMPl3ELL ANALYTICAL INC Tele 51.0-798-1620 Fax 510-798-162162 <br /> ' Advanced GeoEmuonmental,Inc Client Project lD Stephens Marine Date Sampled 11/25/96 <br /> 1803 West March Lane, Suite A Date Received 11/26/96 <br /> ' Stockton, CA 95207 Client Contact Bill Little Date Emracted 11/26/96 <br /> Client P O Date Analyzed 11/27/96 <br /> R <br /> ' Metals <br /> EP4anakt)calmethods 601012007 2392 <br /> Lab ID Client ID Matri\ F)draction° Cadmium Chromium Lead Nickel Zinc Siher %Rec <br /> Surrogate <br /> 71599 I-1 S TTLC ND 33 I 110 I 29 1 190 43 101 <br /> 71600 1-2 S TTLC NTD 26 77 32 56 ND 100 <br /> i <br /> l <br /> 1 Reporting Limit unless S TTLC 0 5 mgkg 05 I 30 20 10 10 <br /> othevAise stated,\D <br /> means not detected W TTLC 0005mgL 0005 0005 005 005 001 <br /> ' abo%e the reporting limit <br /> STLC,TC LP 0 01 mg L 005 02 005 0 05 005 <br /> • soil samples and sludge are reported m mg kg,and%Nater samples and all STLC R TCLP extracts to mglL <br /> ' Lead is analysed using EP 4 method 6010(ICP)for coils,STLC&TCLP extracts and method 239 2(AA Furnace)for i;ater samples <br /> °EPA extracuon methods 1311(TCLP),301013020(Nater,TTLC),3040(organtc matnces,TTLC), 3050(solids,TTLC),STLC from CA Title <br /> 22 <br /> ' 0 surrogate diluted out of range,N/A means surrogate not applicable to this anahsis <br /> It reporting limit raised due matrix interference <br /> i) liquid sample that contains greater than -- 2 vol % sediment, this sediment is extracted %Nuh the liquid, in accordance u71h EPA <br /> methodologies and can significantly effect reported metal concentrations <br /> ' DHS Certification No 1644 Edward Hamilton,Lab Director <br />