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Tes ������ 819 Sinker Avenue 8 <br /> Sacramento CA 95834 <br /> (916}921-961-96 00 <br /> FAX(916)921-0100 <br /> ANALYTICAL TESTING CORPORATION www testamencalnc com <br /> • <br /> Blaine Tech Services(Shell) Project Shell 1 160 West Yosemite Ave,Manteca 5606541 <br /> 1680 Rogers Avenue Project Number 97422510 SAP#168801 Reported <br /> San Jose CA,95112 Project Manager Jason Brown 07/12/06 16 25 <br /> Gasohne\BTEXIOxygenates by EPA method 8260B- Quality Control <br /> TestAmerica- Sacramento,CA <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Lural Units Level Result %REC Lmuts RPD Limit Notes <br /> Batch 6070059-EPA 5030B [P/T1/EPA 8260B <br /> Blank(6070059-BLK3) Prepared&Analyzed 07/10/06 <br /> Ethanol ND 50 ug/l <br /> Tett-butyl alcohol ND 5 0 " <br /> Methyl tert butyl ether ND 050 <br /> Di-isopropyl ether ND 20 <br /> Ethyl tert-butyl ether ND 20 <br /> Tert amyl methyl ether ND 20 <br /> 1 2 Dichloroethane ND 050 " <br /> 1 2-Dibromoethane(EDB) ND 050 <br /> Benzene ND 050 " <br /> Ethylbenzene ND 050 " <br /> Toluene ND 050 " <br /> 46lenes(total) ND 10 <br /> soline Range Organics(C4-C12) ND 50 " <br /> Surrogate 12-DCA-d4 941 100 94 60-140 <br /> Surrogate Toluene-d8 105 100 105 60-140 <br /> Surrogate 4-BFB 902 100 90 60-140 <br /> Laboratory Control Sample(6070059-BSI) Prepared&Analyzed 07/06/06 <br /> Toluene 147 050 ug/I 188 78 70-130 <br /> Gasoline Range Organics(C4-C 12) 1850 50 2200 84 70-130 <br /> Surrogate 12 DCA d4 922 100 92 60-140 <br /> Surrogate Toluene d8 102 100 102 60-140 <br /> Surrogate 4-BFB 977 100 98 60-140 <br /> Laboratory Control Sample(6070059-BS2) Prepared&Analyzed 07/06/06 <br /> Methyl tent butyl ether 167 0 50 ugll 200 84 60-140 <br /> Benzene 18 4 050 200 92 70-130 <br /> Toluene 204 0 50 200 102 70-130 <br /> Surrogate 12-DCA-d4 940 100 94 60-140 <br /> Surrogate Toluene-d8 107 100 107 60-140 <br /> Surrogate 4-BFB 100 100 100 60-140 <br /> I <br /> TestAmenca-Sacramento,CA The results in this report apply to the samples analyzed in accordance with the chain of <br /> • custody document Unless otherwise stated results are reported on a wet weight basis <br /> This analytical report must be reproduced in its entirety <br /> Page 6 of 9 <br /> i <br />