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S U R R O G A T E R E COVE R 1 E 5 R E P O R T Job Number 992707 Report Date 01/06/2000 CUSTOMER IT Group PROJECT- Southland - Martinez ATTN Rhonda Teicheira Method Volatile Organics by GC/MS Batch 10423 Method Code 8260OX Analyst - am Surrogate Units Dibromofluoromethane ug/L Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time 992556-6 Solid 1 23 48 25 000 93 9 60-160 12/07/1999 1442 992556-6 Solid MS 23 57 25 000 94 3 60-160 12/07/1999 1705 992556-6 Solid MSD 24 61 25 000 98 4 60-160 12/07/1999 1740 992648-1 Solid 1 26 37 25 000 105 5 60-160 12/27/1999 0338 992648-1 Solid MS 26 11 25 000 104 4 60-160 12/27/1999 0730 992648-1 Solid MSD 25 45 25 000 101 8 60-160 12/27/1999 0803 LCS 1 25 59 25 000 102 4 57-162 12/31/1999 0204 992707-3 Solid 1 27 75 25 000 111 0 60-160 12/31/1999 0309 992707-4 Solid 1 26 82 25 000 107 3 60-160 12/31/1999 0342 992707-5 Solid 1 25 95 25 000 103 8 60-160 12/31/1999 0414 -Q22710-2 Solid 1 26 99 25 000 108 0 60-160 12/31/1999 0447 10-3 Solid 1 25 88 25 000 103 5 60-160 12/31/1999 0519 110-4 solid 1 26 18 25 000 104 7 60-160 12/31/1999 0552 992710-7 Solid 1 25 77 25 000 103 1 60-160 12/31/1999 0624 992710-8 Solid 1 26.14 25 000 104 6 60-160 12/31/1999 0657 992710-9 Solid 1 25 43 25 000 101 7 60-160 12/31/1999 0729 992709-3 Solid 1 27 25 25 000 109 0 60-160 12/31/1999 0802 992709-4 Solid 1 26 46 25 000 105 8 60-160 12/31/1999 0834 992709-7 Solid 1 26 78 25 000 107 1 60-160 12/31/1999 0907 MB 1 25.64 25 000 102 6 57-162 12/31/2099 0236 Method Volatile Organics -Aromatics Batch 10428 Method Code 8020BX Analyst evd Surrogate Units 4-Bromofluorobenzene ug/L l Lab ID Matrix QC Type Dilution Result True Value Percent Recovery Limits Flag Date Time LCS 1 41.45 50 0000 82 9 64-147 01/04/2000 1642 LCO 1 43 19 50 0000 86 4 64-147 01/04/2000 1708 MB 1 40 98 50 0000 82 0 64-147 01/04/2000 1800 992709-4 Solid MS 1 44 45 50 0000 88 9 64-147 01/04/2000 1944 992709-4 Solid MSD 1 41 81 50 0000 83 6 64-147 01/04/2000 2010 992693-7 Solid 1 41.16 50 0000 82 3 64-147 01/04/2000 2036 992693-11 Solid 1 39 76 50 0000 79 5 64-147 01/04/2000 2128 992693-12 Solid 1 41 49 50 0000 83 0 64-147 01/04/2000 2153 992693-14 Solid 1 42 98 50 0000 86 0 64-147 01/04/2000 2219 992693 40 Solid 1 40 51 50 0000 81 0 64-147 01/04/2000 2245 992693-45 Solid 1 40.27 50 0000 80 5 64-147 01/04/2000 2311 #09-3 93-48 Solid 1 38 85 50 0000 77 7 64-147 01/04/2000 2337 93-52 Solid 1 40 99 50 0000 82 0 64-147 01/05/2000 0002 Solid 1 40 92 50 0000 81.8 64-147 01/05/2000 0211 992709-4 Solid 1 32 34 50 0000 64.7 64-147 01/05/2000 0821 1 Page 13 1 i I