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02/27/2001 11 18 209467111 AGE STOCKTON PAGE 08 <br /> bent by McCampbell Analytical, Ilp 1 925 798 4812, Feb-9-01 0 20PM, Page 9112 <br /> 1 <br /> I <br /> MCCAMP$ELL ANALYTICAL INC10 2nd Avenue South,ND7,Pacheco,CA 94553-5560 <br /> • C Telephone 925-798-1620 1 a 925-798-1622 <br /> h,ttlii'.—mccarnpbeil i.om Ir Head main 9mccampbelt i,am <br /> Advanced GeoEnvuonmetttal C tent Project TO Ratn Water C'tir wash € Date Sampled 01/31/01 <br /> 837 Shaw Road I Date Reeetved 02/01,Ol ^I <br /> Stockton CA 95215 (;beset Contact Tim CuellarDate 1Ix>xacted 02,'01-02/08/01 <br /> .1 V Clens F D f hate Analy.d 02,01-02/()&O1 <br /> EPA mctlWd 8260 volatile Organics By GC/MS <br /> Lab ID �1211C tent 1D K <br /> Matnx W <br /> Cornpound (ancontrattnns lk mOn-na Limn Compound y Agrmu,8 Limn <br /> �, 9 p Cunccnlrrt+tm <br /> �eet0lx ' - Nt7«5Q 5D 25 iron9-1 3-Dialuropropcne 171)<350 f 0 50 <br /> tsn2Crn 3 G0 " 1 0 5 0 f 5,Y? dibmnnde N1Y 50 i 0 J0 <br /> r0mnberttene NV"J5 --T-0 -3-0 5 0 E,tb l ize))c Nt?<15[1 1 5 0 <br /> Ammee loromethant NID[350 —10 U F(exachlprabutsd,enc NEK1R0 yl-D-- 25 <br /> Itrotnodichltxnntethtmc NJ){350 -7—o -To-- to nntctbane U< 50 t 0 5 0 <br /> I1mmOtvrm 961350 t S 0 U lanpropy enzeneV UK SO 10 s Q <br /> RromamethanC 1\UG1S0 1-0 S 0 P Tsopmpvltriluene N17<35U 10 50 <br /> n-Butyl benzene 1Vr)c350 1 0 S U Methyt butyl X,:tane' 1vl):15G 1-0 5 U <br /> ace-BUtyT benzene NU<350 1-0 S c ylt na Chlunde N[x990 10 5 A <br /> tus-Butyl benzene N 50 —F 4 5 0 Methyl ethyl keionc` Nl?c350 -z—D I0 <br /> LarhO0Lht u 1dc NrK350 —1() <br /> 4 0 Me[!t}I rtttbuty &ttunc NL>C350 1 0 S 0 <br /> • CarbOn Tetrachlundc NT]<35(1 1 U 5 U Mdhyl krt-HUry Lthcr{h1 lBE) (q S(1 <br /> Chlorohenzcne 354 1 U_ S 0 Niphtholrnc 1�1}�5U 5 0 5 0 <br /> 7c[hune >`1Y350 1 0 S 0 n- ropy]benzene Ntyc350 10 50 <br /> 2CjQr4)Cthy1 V ntyl l=ute N11C150 l 0 5 0 S[yre+ie Ac35U 1 0 5 t) <br /> Chlorr,fbrm Nt)<1SU 10 50 l,l,i,2Tetraelllurncrnane L) 1$0 Ifl s0 <br /> Ch(urOnrtharte ND<350 10 i 0 I,i,2-,-rLtar-hlaoc bane Nfk 50 1 0 50 <br /> 2- loroluluenz NA 0 1-0 --f—O letrachloroethtne NfbC350 : 0 so <br /> 1 Ch orotoluont: NUc350 —10 5 0 TolUcne N1y.350 10 50 <br /> Dtbrumoehlgromethanc TvE]c350 1 U 5 1 2,3-Tnthlorobdnzena Nt}e35U Sq 15 <br /> 1 2-Dibromo-3.hlotupropanc. Np<1$V 2 0 10 7,2,q rtchlom rnLtnc \UClsll 5 0 25 <br /> 01hromomethanc ND-35U 1-0 50 1,1, -Trichlorue[hanc Nps SU l0 J0 <br /> 12 l]ichlorabenrene Nfyc35U 1-0 S U 1,1 2-TnehlarUelhenc NDr3S0 1 0 To <br /> 1 3- ichlorohrriM- ND <br /> nc WU<350 E 0 S U [nehlotoethrne ND<350 --1-0- <br /> 350 <br /> 0 S V <br /> 1 4 Drchna lwll<350 I O S U IriC nroflUurorOethane RD 350 l 0 5 0 <br /> � erl+ane x35npropanIU1,l- is Lk350 1 SU 12 4 Tnrnelhyl Irene VD�350 10 5 0 <br /> ND<150 l0 S 0 1.3,5-TilMe ylbcnzcnc )�1r11350 1U 5 U <br /> 1,1-t7tcltND<350 1 0 5 0 Vtnv Acetate 1\tk350 50 25 <br /> cts-I,2Dhcnc N 150 1 50 Vmvl hlorrde'"uanx-1,2cthcn� ND< 10 5V ,ylcnca total 5Z350 —10 5 U <br /> ( 2-Dlchlnrupropano Nth3gU 1 0 50 (bruntcttur <br /> 1,3-DichloropTupene NrK350 l 0 50 Surropattc l emiocries(%) <br /> 2,2 Oicb mpropnne N1JCl 4 10 _ 0 0[hntrnoJ1U(rcutncthinc 74 <br /> t-01c omprotwna NUc SU I 50 Toluene 8 102 <br /> CIA-1,11 is luropropcnc 'Dc350 I 0 5 0 q- ramot unrpbenzcm 101 <br /> 'Aatrt and raper sarnples are reMrred In ug/L surl and sludge samples,n UVkS,ik'PC r in ue,"rc ani all Tt I p/SPt P cxunt.ts rn ug/l <br /> Ni)manna not dttectcd ahuve the reporting Omit N/A moans enulyte not applieQbie to[hi'2naly.is <br /> (b) 3-propanune or dinxthy) ketone, (c) (.-Lhlnrpethaxy)cthene (d)2 hecunont (c)dMIlletrorrretlianc (rl 2 humnortc (a)4 methyl-2 <br /> penranonc yr IsoprOpwlacci,)ne (Is)hghter than cater immiscible sheen +a pi Osenr (r)114111d s¢mplc thut eO"Wrl%9 arr than -S vo( % <br /> aedinlcnt, (3) sample d+l sted dvc to hrgh organic content (L) erlienylbcncene (1) meth>ihcnrene, (m)34ctzc acid ethenyl ester (n) <br /> chlmaethcne (O)dtme[hylbcrvcncs <br /> D Ceruficatton No 1644 Fdward Hamilton, Lab Ditectrr <br />