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r110 2nd Avenue South #iD7,Pacheco,CA 94553-5560 <br /> LMcCampbell Analytical Inc Telephone 925-798-1620 Fax 925-798-1622 <br /> h //www mccampbell com E mail rmin@mc:carnpbell cam <br /> rAdvanced GeoEnvironmental;Inc Client Project ID Raul Water Car Wash Date Sampled 07/23/03 <br /> • 837 Shaw Road Date Received 07/24/03 <br /> rStockton, CA 95215 Client Contact Tim Cuellar Date Extracted 07/24/03 <br /> ' Client P O -J Date Analyzed 07/24/03 <br /> Lead by Graphite Furnace Atomic Absorption* <br /> xtraeuon method E20t19 Analytical methods E200 9 Work Order 0307420 <br /> Lab ID Client ID Matrix Extraction Lead DF %SS <br /> 0307420-002D EFFLUENT W TTLC ND 1 N/A <br /> r <br /> r <br /> r <br /> r <br /> r� <br /> r <br /> r <br /> r <br /> I <br /> Reporting famrt for DF=1, W 17LC 0 005 mg/I. <br /> r ND means not detected at or <br /> above the reporting limit S TTLC NA mg/kg <br /> I <br /> "'water/product/oil/non-aqueous liquid samples and all TCLP/STLC/DISTLC/SPLP extracts are reported in mg/L,soillsludge/solid samples in mg/kg, <br /> ' wipe samples inµglwipe,filter samples inµg/filter <br /> #means surrogate recovery outside of acceptance range due to matrix interference,&means low or no surrogate due to matrix interference,ND means not <br /> detected above the reporting limit,N/A means not applicable to this sample or instrument <br /> ' Analytical Methods EPA 6010C/200 7 for all elements except 200 9(water/liquid-Sb,As,Pb,Se TI),245 1 (Hg),7010 <br /> (sludge/soil/solid/oil/product/wipe/filter-As,Se,TI),7471H(Hg) <br /> i)liquid sample that contains greater than—2 vol %sediment,this sediment is extracted with the liquid,in accordance with EPA methodologies and can <br /> significantly effect reported metal concentrations,j)reporting limit raised due to insufficient sample amount,k)results are reported by dry weight,y) <br /> estimated values due to low surrogate recovery,z)reporting limit raised due to matrix interference <br /> , <br /> � I , <br /> DHS Certification No 1644 f Angela Rydelius,Lab Manager <br />