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CLIENT: Pacific Edge Engineering ANALYTICAL QC SUMMARY REPORT <br /> Work Order: N023518 <br /> Project: Manteca Firing Range, 0025 TeatCOde: 7471_S <br /> Sample ID MB-61641 SampType: MBLK TestCode: 7471_S Units: mg/Kg Prep Date: 3/21/2017 RunNo: 114198 <br /> Client ID: PBS Batch ID: 61641 TestNo: EPA 7471A Analysis Dale: 3/21/2017 SegNo: 2597636 <br /> Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qua[ <br /> Mercury NO 0.10 <br /> Sample ID LCS-61641 SampType: LCS TestCode: 7471_S Units: mg/Kg Prep Date: 3/21/2017 Runblo: 114198 <br /> Client ID: LCSS Batch ID: 61641 TestNo: EPA 7471A Analysis Dale: 3/21/2017 SegNo: 2597637 • <br /> Analyte Result PQL SPK value SPK Ref Val %REC LowUmit HighLimit RPD Ref Vel %RPD RPDLImit Qual <br /> Mercury 0.444 0.10 0.4167 0 107 80 120 <br /> Sample ID N023510-002A-MS SampType: MS TestCode: 7471_S Units: mg/Kg Prep Date: 3/21/2017 RunNo: 114198 <br /> Client ID: ZZZZZZ Batch ID: 61641 TestNo: EPA 7471A Analysis Date: 3/21/2017 SegNo: 2597638 <br /> Analyte Result PQL SPK value SPK Ref Val %REC Lowt-imit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> Mercury 0.641 0.099 0.4126 0.2421 96.6 75 125 <br /> Sample ID N023610-002A-MSD SampType: MSD TestCode: 7471S Units: mg/Kg Prep Dale: 3/21/2017 RunNo: 114198 <br /> Client ID: ZZZZZZ Batch ID: 61641 TestNo: EPA 7471A Analysis Date: 3/21/2017 SegNo: 2597639 <br /> Analyte Result PQL SPK value SPK Ref Val %REC LowLimit HighLimit RPD Ref Val %RPD RPDLimit Qual <br /> Mercury 0.536 0.10 0.4160 0.2421 70.8 75 125 0.6413 17.8 20 S <br /> Qualifiers: <br /> B Analyte detected in the associated Method Blank E Value above quantitation range H Holding times for preparation or...lysis exceeded <br /> 1 Analyte detected below quantitation❑mutes NO Not Detected at the Reporting Linut R RPD outside accepted recovery lintits <br /> adola SSpike/Surrogate outside of limits due to matrix interference DO Surrogate Diluted Out Calculations are based on raw values <br /> CAUFORNIAI P:562.219.7435 F:M2.219.7436 NEVAOAIP:702.307.2659 F:M2.307.269' <br /> A55ET 1A90RATORIE5 11110 Artesia BIW.,Ste B,Cerritos,CA 90703 3151 W.Pori Rd.,Las Vegas,NV 89118 <br /> ELAP Cart 2921 ELAP Cert 2676 I NV Cert NVDN22 <br /> 3iarWna Glsnb with Pa.aion and Prufenulnrulltars- EPA 10 CA01638 ORELAP/NELAP Cart 4046 <br /> Page 99 of 99 <br />