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Cal if omnia Duper lmunL U lox is SUb5tallLes Lwin of nm efJo., m : v umiu <br /> Hazardous Materials Laboratory to 4!0600 <br /> Inorganic Section <br /> Quality Assurance Summary for ICP <br /> HML Soil QC Sample Method Calibration Verification Duplicate Spiked Sampte HML No.: 960799 Matrix: SOIL <br /> Blank Standard <br /> Element Spike Results mg/kg Unspiked Spike X Recovery <br /> /k m /L Result Added <br /> found known X m9/L found known % A: B: RPD (mg/kg) (mg/kg) A: 6: <br /> As-Arsenic 52.4 63.3 82.8 0.99 10.0 9.9 516 476 8.57 29.4 500 97.3 89.3 <br /> Ba-Barium 39.9 44.7 89.3 1.03 10.0 10.3 639 624 2.87 109 500 106 103 <br /> Be-Ber Ilium 18.1 21.5 84.2 0.20 2.00 10.0 98.2 94.8 3.54 0.40 100 97.8 94.4 <br /> Cd-Cadnium 22.0 25.5 86.3 0.97 10.0 9.7 459 443 3.56 1.87 500 91.4 88.2 <br /> Co-Cobalt 17.2 20.7 83.1 0.99 10.0 9.9 475 459 3.49 8.74 500 1 93.2 90.0 <br /> Cr-Chromium 50.7 59.6 1 85.1 0.93 10.0 9.3 Results are above the calibration curve <br /> Cu-Copper 31.2 37.7 82.8 1.05 10.0 10.5 1932 1760 31.5 1305 500 125 91.0 <br /> Mo-Molybdenum 17.1 30.3 56.4 0.98 10.0 9.8 427 396 7.62 4.40 500 84.5 78.3 <br /> Ni-Nickel 29.3 35.4 82.8 0.97 10.0 9.7 1321 1168 39.4• 856 500 93.0 62.4 <br /> Pb-Lead 26.2 31.0 84.5 0.97 10.0 9.7 520 481 9.03 68.6 500 90.3 82.5 <br /> Se-Selenium 64.1 72.8 88.0 1.02 10.0 10.2 502 480 4.66 8.25 500 98.8 94.3 <br /> Tl-Thalti um 111 125 88.8 0.98 10.0 9.8 461 444 3.76 <7.50 500 92.2 88.8 <br /> V-Vanadium 29.1 40.9 71.1 0.99 10.0 9.9 475 466 1.96 12.1 500 92.6 90.8 <br /> Zn-Zinc 39.1 46.3 84.4 0.82 10.0 8.2 1699 1475 72.5• 1278 500 84.2 39.4 <br /> HML Liquid OC Sample Reagent Inorganic Ventures Duplicate Spiked Sample HML No.: 960789 Matrix: LIQUID <br /> Blank Reference Standard <br /> Element ng/kg mg/L Spike Results mg/kg Unspiked Spike X Recovery <br /> Result Added <br /> found known % found known X A: B: RPD (mg/kg) (mg/kg) A: B: <br /> /L <br /> As-Arsenic 2.59 3.01 86.0 <0.04 1.01 1.00 101 95.5 95.8 0.31 <0.40 100 9S.S 95.6r':�L':i'- <br /> Ba-Barium 2.95 3.01 98.0 0.002 1.04 1.00 104 98.2 93.6 4.80 0.13 100 98.1 93.7 <br /> Be-Ber Ilium 0.76 0.85 89.4 <0.001 0.20 0.20 100 18.3 18.6 1.63 <0.01 20.0 91.5 - 93.0 <br /> Cd-Cadmium 1.99 2.47 80.6 <0.004 0.96 1.00 96.0 86.1 87.3 1.38 0.04 100 86.1 87.3 <br /> Co-Cobalt 2.06 2.43 84.8 <0.02 0.99 1.00 99.0 89.2 89.3 0.11 <0.20 100 89.2 89.3 <br /> Cr-Chromiun 4.52 5.39 83.9 <0.03 0.96 1.00 96.0 88.3 83.0 6.44 3.41 100 84.9 79.6 <br /> Cu-Copper 28.6 29.0 98.6 0.019 1.10 1.00 110 113 119 6.44 22.9 100 90.1 96.1 <br /> Mo-Molybdenum 1.77 1.97 89.8 <0.03 0.99 1.00 99.0 92.5 90.7 1.97 <0.30 100 92.5 90.7 <br /> Ni-Nickel 4.01 4.96 80.8 <0.03 0.97 1.00 97.0 120 122 2.30 34.1 100 85.9 87.9 <br /> 'I <0.50 100 87.9 91.6 <br /> I Pb-Lead 8.45 10.2 82.8 <0.05 0.99 1.00 99.0 87.9 91.6 4.12 <br /> Se-Selenium 3.01 3.47 86.7 <0.08 1.02 1.00 102 94.7 95.6 0.95 <0.80 100 94.7 95.6 <br /> / j Tl•Thalliun 8.95 10.1 88.6 <0.15 0.99 1.00 99.0 90.9 90.5 0.44 <1.50 100 90.9 90.5 <br /> V-Vanadium 2.28 2.49 91.6 <0.03 1.00 1.00 100 91.1 89.2 2.11 <0.25 100 91.1 89.2 <br /> Zn-Zinc 47.2 57.1 82.7 <0.015 1.01 1.00 101 127 129 2.18 4 100 90.6 92.6 <br /> NOTE: ` = High RPD due to hetero eneity of the s mp S. / <br /> ICP Analyst's Signature: !CL � C, Milad S. Iskander, Supervisor: Date:� <br /> Chemist: Zaida R. ILejay Chemist's Signature:��/Zc.,{',y, "fe, cr,... _ - - - - - <br /> Date Analyzed: 2/11/97 j <br />