ARCHIVED REPORTS_2011 4TH QUARTER MONITORING

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_ - - El`NIROnMENTAL -11-0 . . . - Analytical Chemists _ db www.fglinc.com '► .� January 10, 2012 Lab ID : STK 1151166 Musco Family Olive Environmental Customer : 3-11544 Quality Control-Inorganic Constituent Method Date/ID Type Units Conc. QC Data DQO Note Metals Sodium 200.7 MS mg/L 12.50 102% 75-125 (SP 1 1 13 352-00 1) MSD mg/L 12.50 99.3% 75-125 MSRPD m 798.8 0.3% <20.0 200.7 12/29/11:219141 AC CCV ppm 25.00 99.7% 90-110 CCB ppm -0.04 1.0 CCV ppm 25.00 101% 90-110 CCB ppm -0.05 1.0 Wet Chem Solids,Total Dissolved 2540 G 12/27/11:214251CHL Blank mg/L ND <20 LCS mg/L 995.0 98.8% 90-110 (STK 1151181-003 Dup m 0.6% 10.0 Solids,Suspended 2540G 12/22/11:31202OCTH Blank mg/kg ND <1 LCS mg/kg 500.0 98.4% 38-138 LCS mg/kg 500.0 97.6% 38-138 (STK 1151159-002 Du m 0.9% 28.7 Nitrogen,Total Kjeldahl 351.2 12/28/11:214303caa Blank mg/L ND LCS mg/L 12.00 100% 41-148 MS mg/L 12.00 101 % 25-149 (STK 1151143-003) MSD mg/L 12.00 151% 25-149 435 MSRPD mg/L 12.00 39.0% <25.7 435 itrate+Nitrite as N 450ONO3F MS mg/L 4.000 172% 5-285 (CC 1183403-001) MSD mg/L 4.000 167% 5-285 MSRPD mg/L 4.000 0.7% <30.4 MS mg/L 4.000 70.4% 5-285 (STK 1151166-002) MSD mg/L 4.000 77.6% 5-285 MSRPD mg/L 4.000 9.6% <_30.4 450ONO3F 12/29/11:219093AMB CCB mg/L -0.013 0.1 CCV mg/L 4.000 93.6% 90-110 CCB mg/L -0.004 0.1 CCV mgiL 4.000 90.0% 90-110 OD 5210B 12/22/11:300885SA RgBlk mg/L 0.05 2 RgBlk mg/L 0.14 2 LCS mg/L 198.0 91.4% 84.6-115 (STK1151164-001) Dup mg/L 6.7% 15.9 (STK 1151164-001) m 11.2% 15.9 5210B 12/27/11:300916SA CCV m 1.000 99.0% 80-120 Nitrogen,Total Kjeldahl EPA351.2 12/29/11:219063AMB CCB mg/L 0.276 0.5 CCV mg/L 1.000 103% 90-110 CCB mg/L 0.176 0.5 CCV mg/L 1.000 103% 90-110 Definition CCV :Continuing Calibration Verification-Analyzed to verify the instrument calibration is within criteria. CCB :Continuing Calibration Blank-Analyzed to verify the instrument baseline is within criteria. Blank :Method Blank-Prepared to verify that the preparation process is not contributing contamination to the samples. RgBlk :Method Reagent Blank-Prepared to correct for any reagent contributions to sample result. LCS :Laboratory Control Standard/Sample-Prepared to verify that the preparation process is not affecting analyte recovery. MS :Matrix Spikes-A random sample is spiked with a known amount of analyte.The recoveries are an indication of how that sample matrix affects analyte recovery. MSD :Matrix Spike Duplicate of MS/MSD pair-A random sample duplicate is spiked with a known amount of analyted.The recoveries are an indication of how that sample matrix affects analyte recovery. Dup :Duplicate Sample-A random sample with each batch is prepared and analyzed in duplicate.The relative percent difference is an indication of precision for the preparation and analysis. MSRPD :MS/MSD Relative Percent Difference(RPD)-The MS relative percent difference is an indication of precision for the preparation and analysis. ND :Non-detect-Result was below the D O listed for the analyte. Page 9 of 11 Corporate Offices&Laboratory Office&Laboratory Offlce&Laboratory Office&Laboratory Field Office 853 Corporation Street 2500 Stagecoach Road 563 E.Lindo Avenue 3442 Empresa Drive,Suite D Visalia,California Santa Paula,CA 93060 Stockton,CA 95215 Chico,CA 95926 San Luis Obispo,CA 93401 TEL:559/734-9473 TEL:805/392-2000 TEL:209/942-0182 TEL:530/343-5818 TEL:805/783-2940 Mobile:559/737-2399 FAX 805/525-4172 FAX:209/942-0423 FAX:530/343-3807 FAX:805/525-4172 FAX:559/734-8435 CA NELAP Certification No.01110CA CA ELAP Certification No. 1563 CA ELAP Certification No.2670 CA ELAP Certification No.2775