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Lancaster <br /> Laboratories Analysis Report <br /> 2425 New Holland Pike PO Box 12425 Lancaster,PA 17605-2425•717 656 2300 Fax 717 656-2681•www lancasterlabs corn <br /> Page 3 of 3 <br /> Quality Control Summary <br /> Client Name ChevronTexaco Group Number 858712 <br /> Reported 07/18/03 at 02 58 PM <br /> Surrogate Quality Control <br /> Limits 81-120 82-112 85-112 83-113 <br /> Analysis Name BTEX+5 Oxygenates+EDC+EDB+ETOH <br /> Batch number P031921AA <br /> Dibromofluoromethane 1,2-Dichloroethane-d4 Toluene-de 4-Bromofluorobenzene <br /> 4076851 93 92 104 94 <br /> Blank 93 93 103 94 <br /> LCS 94 93 102 101 <br /> Ms 93 94 101 100 <br /> MSD 93 96 102 100 <br /> Limits 81-120 82-112 85-112 83-113 <br /> *-Outside of specification <br /> (1) The result for one or both determinations was less than five times the LOQ <br /> (2) The background result was more than four times the spike added <br />