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f <br /> Superior Precision Ana/yr-ica/, /nc_ <br /> . •enc scc �.,;�for:, 2.. . - f S- 6-7 2003 f ��� �� <br /> 5. .2 . 72 <br /> C E R T I F I C A T E O F A N A L Y S I S <br /> LABORATORY NO. 54118 DATE RECEIVED: 09/24/91 <br /> CLIENT : Canonie Environmental DATE REPORTED: 09/30/91 <br /> CLIENT JOB NO. : 91-106-02 <br /> ANALYSIS FOR BENZENE, TOLUENE, ETHYL BENZENE & XYLENES <br /> by EPA SW-846 Methods 5030 and 8020 <br /> TAB Concentration(mg/kg) <br /> # Sample Identification Ethyl <br /> -- Benzene Toluene Benzene Xylenes <br /> 1 025-TP2-SW15 4 . 0 150 79 520 - <br /> 2 025-TP3-SW15 . 5 0 . 21 11 5 . 6 41 <br /> 3 025-TPI-NE16 ND<0 3 3 . 0 1 . 3 9 . 6 <br /> 4 025-TP2-NE16 <br /> 5 025-TP3-NE16 . 5 8 . 9� 270 100 730 <br /> 6 025-SP-1 0 . 98 22 7 . 8 58 <br /> 7 025-SP-2 ND<0 . 3 22 24 230 <br /> 8 025-SP-3 ND<0 . 3 2 . 8 2 . 0 20 <br /> 9 025-SP-4 0 . 30 0 . 26 0 . 085 3 . 1 <br /> 10 025-SP-5 ND< . 003 ND< . 003 ND< . 003 ND< . 00 <br /> 025-SP-6 ND< . 003 0 . 23 0 . 11 0 . 39 <br /> 035-TP2-E12 .5 ND< . 003 0 . 005 ND< . 003 ND< . 003 ~ , <br /> 13 035-TP2-C13 ND< . 003 0 . 010 ND< . 003 ND< . 003 <br /> 4 035-TP3-E13 .5 ND< . 003 ND< . 003 ND< . 003 ND< . 003 <br /> 5 035-TP3-W14 ND< . 003 0 . 004 ND< . 003 0 . 009 <br /> 16 035-TP2-W14 . 5 ND< . 30 1 . 6 1 . 7 15 <br /> 17 035-TP1-W14 ND< . 003 0 . 015 ND< . 003 0 . 014 <br /> 8 035-TP1-E13 . 5 ND< . 003 ND< . 003 ND< . 003 0 . 005 <br /> 19 035-PUMP1--3 . 5 ND< . 003 ND< . 003 ND< . 003 ND< . 003 <br /> 20 035-PUMP2-4 . 5 24 400 160 1200 , <br /> 1 035-SP-1 4 .2 56 21 160 <br /> 2 035-SP-2 1 . 1 14 5 . 3 44 <br /> 23 035-SP-4 0 .49 55 3 . 9 490 <br /> 4 035-SP-3 ND<0 . 30 7 . 7 1 . 0 430 <br /> 5 035-SP-5 ND<0 . 30 3 . 0 0 .44 74 <br /> 26 035-SP-6 37 490 150 1400 <br /> )7 025-TP3-SW20 ND<0 . 30 41 11 120 <br /> i«g/kg - parts per million (ppm) <br /> Minimum Detection Limit in Soil : 0. 003 mg/kg <br /> QAQC Summary <br /> } Daily Standard run at 20ug/L. %DIFF 8020 = < 15% <br /> MS/MSD Average Recovery = 91% : Duplicate RPD = 2 .2% <br /> s <br /> Richard Srna, Ph.D. <br /> Com) <br /> Labor to rector <br /> Cer[Ified Leboratones <br />