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COLUMBIA ANALYTICAL SERVICES,INC <br /> QA/QC Report <br /> Bent ARCO Products Company Service Request L9901977 <br /> rolect WA##24406 00/6020-Manteca Date Collected NA <br /> Sample Matrix Soil Date Received NA <br />' Date Extracted NA <br /> Date Analyzed 511199 <br /> Matnx Spike/Duplicate Matrix Spike Summary <br /> Oxygenates <br /> gJampleName T-2-S(16') Units ug/Kg(ppb) <br /> 4ab Code L9901977-007MS L9901977-007DMS Basis Wet <br /> est Notes <br /> I <br /> Percent Recovery <br /> CAS Relative <br /> Prep Analyses Spike Level Sample Spike Resent Acceptance Percent Result <br /> Inalyte Method Method MRL MS DMS Result MS DMS NLS DMS Lumts Difference Notes <br /> Benzene EPA 5030 8260 0 5 100 100 ND 10 5 114 105 114 66-142 8 <br /> tluene EPA 5030 8260 05 100 100 ND 106 148 106 148 59-139 33 A4 <br /> ylbenzene EPA 5030 8260 0 5 100 100 ND 102 120 102 120 60-130 18 <br /> r <br /> 1 <br /> I <br /> t <br /> 1 <br /> 14 Outside of acceptance limits The LCS was acceptable,therefore,data was approved <br /> i f�' <br /> Approved By -" J Date r r 9 <br /> Page No <br /> 01977VOAHWI DMS(2)514/99 <br />