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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: 2019 Annual Fly Ash Profiling <br /> 2526 W.Washington St. Project Number: 4701254256 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 04/12/19 16:16 <br /> Total Recoverable Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A]D0085-EPA 7471A <br /> LCS Dup(A]D0085-BSD1) Prepared:04/08/19 Analyzed:04/09/19 <br /> Mercury 0.214 0.016 mg/kg 0.200 107 80-120 2.94 20 <br /> Matrix Spike(A]D0085-MS1) Source:1904027-01 Prepared:04/08/19 Analyzed:04/09/19 <br /> Mercury 0.226 0.016 mg/kg 0.200 0.0102 108 75-125 <br /> Matrix Spike Dup(A]D0085-MSD1) Source:1904027-01 Prepared:04/08/19 Analyzed:04/09/19 <br /> Mercury 0.234 0.016 mg/kg 0.200 0.0102 112 75-125 3.13 20 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 11 of 18 <br />