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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: 2019 Annual Fly Ash Profiling <br /> 2526 W.Washington St. Project Number: 4701254256 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 04/12/19 16:16 <br /> STLC Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A]D0106-EPA 7470A <br /> Matrix Spike(A]D0106-MS1) Source:1904020-01 Prepared:04/11/19 Analyzed:04/12/19 <br /> Mercury 0.0315 0.00240 mg/L 0.0400 ND 78.8 75-125 <br /> Matrix Spike Dup(A]D0106-MSD1) Source:1904020-01 Prepared:04/11/19 Analyzed:04/12/19 <br /> Mercury 0.0333 0.00240 mg/L 0.0400 ND 83.2 75-125 5.43 20 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 15 of 18 <br />