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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: 2020 Annual Bottom Ash Profiling <br /> 2526 W.Washington St. Project Number: 4700995195 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffman 04/10/20 21:46 <br /> Sample Integrity WORK ORDER:,-PVD �4 4 <br /> Company Name: <br /> Bate Received- _zA 7 ! 2.6 New Client: Y <br /> Section 1—Sample Arrival Information <br /> Sample Transport: ONT'RAC UPS USPS walk-In ELCi�M Co Fed-Ex Other_ <br /> Transported 1n: Ice Chest opt Hand <br /> Packing materials_ Bubble Wrap Foam Packing Peanuts Paper Other: M Pt' <br /> aas chilling process begun`_' Y Samples Received: Chilled to TouchI bin 1 Cha Ice <br /> Temperature oCSamples(°C): ci t . �+ ._ bce Chest Temperature(s)(°C):> <br /> Section 2—Bottle/Analysis Info. <br /> Yes No N/A Comments <br /> Did ail bottles arrive unbroken and intact? <br /> Did all bottle labels agree with COC? <br /> Were correct containers used for the tests requested? <br /> Were correct preservations used for the tests requested? <br /> Was a sufficient amount of sample sent for tests indicated? <br /> Were bubbles present in VOA Vials?:(Volatile Methods Only) 1 3Z-1 <br /> Section 3-$arama/Flow re uIstor InCormatioa � {� <br /> gleed Srs.rrrruc#= <br /> Unused Summa <br /> Cleanin Summa#: <br /> Re ulatorff: <br /> Was there any visual damage to summa canisters or flow regulators?Explain- <br /> Section 4-COC Information <br /> Yes No Commenrs Yes No Comments <br /> COC Received Analysis Requested r� <br /> Date Sampled > I Samples arrived within holding time <br /> Time Sampled �[ _ �HDld'd�mqeslel,,5 than 72 ho„raSample ID <br /> Rush Turn Around Time 3 DAY Client Contact Information <br /> SHORT HOLD LIST x-72 hours <br /> if Chlariac Comosivi - ColiPpnn Dissolved Ox Odor Nitrate Nitrite <br /> NLBAS TurbidityearsOmr[fmtoonhaKhaNe <br /> 9iacxcmicl Ox nanHPC Color <br /> un reserved <br /> Section 5-Comments I Iliscre ancies <br /> Client notified of discrepancies- Yes I No Notified b <br /> comments,; - <br /> Sin Numbcr/Location: Filled out by: R t a Date_ H 17/ <br /> COC Scmanned/A[iached by; Time- 1�,Sa <br /> Saples labeled by' <br /> Sample+.abets reviewed by: <br /> Excelchem Laboratories.Tnc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2of4 <br />