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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: 2019 Annual Fly Ash Profiling <br /> 2526 W.Washington St. Project Number: 4701254256 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 04/15/19 16:40 <br /> Total Recoverable Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A]D0107-EPA 7471A <br /> LCS Dup(A]D0107-BSD1) Prepared:04/11/19 Analyzed:04/12/19 <br /> Mercury 0.190 0.016 mg/kg 0.200 95.2 80-120 2.90 20 <br /> Matrix Spike(A]D0107-MS1) Source:1904027-01RE1 Prepared:04/11/19 Analyzed:04/12/19 <br /> Mercury 0.206 0.016 mg/kg 0.200 0.0182 94.1 75-125 <br /> Matrix Spike Dup(A]D0107-MSD1) Source:1904027-01RE1 Prepared:04/11/19 Analyzed:04/12/19 <br /> Mercury 0.211 0.016 mg/kg 0.200 0.0182 96.5 75-125 2.30 20 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 11 of 18 <br />