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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: 2019 Annual Bottom Ash Profiling <br /> 2526 W.Washington St. Project Number: 4701254256 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 04/12/19 16:11 <br /> Sample Integrity NVORK ORDER: 1944030 <br /> Date Received:4/05/2019 <br /> See tion 1—Sample Arrival In£o. <br /> Sample Transport: EXCELCI{EA4tCourier Transported in: Box <br /> Describe type of packing materials: NIA <br /> Has chilling process begun? Yes Samples Received: Ambient . <br /> Temperature of Samples('C:): ;r.4 Icc Chest Temperature(s)("C): N1 <br /> Section 2—Bottle/Analysis info. <br /> Yea No NIA Cammcnn <br /> Did ail bottles arrive unbroken and intact? x - <br /> Did all bottle labels agree with COC? x <br /> Were correct containers used for the tests requested? x - <br /> Were correct preservations used for the tests requested? x <br /> Was a sufficient amount of sample sent for tests indicated? x <br /> Were bubbles present in VOA Vials?:(Volatile Methods Only) x - <br /> Section 3—SUmmaMlow regulator InIII <br /> . <br /> V6ed Suacnea.#: _ <br /> Unused Summa#: <br /> Cleaning SummaM: _ <br /> Regulator#- <br /> Was there any visual damage to summa c an inters or flow re uIators?Exp Iain. <br /> Section 4—COC Info. <br /> Cam letncl Info From Completed <br /> Yes No Comment Yes No Comments <br /> Was COC Received K - Analysis Requested x <br /> Date Sampled x - Samples arrived within holding time x <br /> Time Sampled x - Any hold times less than 72 hrs. x <br /> Sample ID X - Client Name X - <br /> Rush TAT It -5 day Address/Telephone# x - <br /> Section 5—Comments/Discrepancies <br /> Was Client notified of discrepancies: N/A Notified by: <br /> Explanations 1 Comments: <br /> r <br /> Samples labeled by: RL Filled out by: Rachele Lang Date:415/2[)19 <br /> BIN; Dept.1 1 Time: 10:14 <br /> COC Scanned/Attached by: RL <br /> Samplc labels reviewed by: RL <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2of2 <br />