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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: 2019 Annual Bottom Ash Profiling <br /> 2526 W.Washington St. Project Number: 4701254256 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 04/15/19 16:45 <br /> Sample Integrity WORK ODDER: 1904048 <br /> Date Received:4/05/201 9 <br /> See tion l—Sample Arrival Into. <br /> Sample Transport: Exi-EtCIIEM Courier "transported In: Hand <br /> Describe type of packing materials: NIA <br /> I las chilling process begun? No Samplcs Received: Ambient <br /> 'temperature of Samples('C): 21.2 ice Chest Temperatures)(°C): N/A <br /> Section 2--BottlelAnalysis Info- <br /> Yes No MIA CDi11 s <br /> Did all bottles arrive unbroken and intact? x - <br /> Did all bottle labels agree with COC? x <br /> Were correct containers used for the tests requested? x - <br /> Were correct preservations used for the tests requested? —x— <br /> Was a sufficient amount o sample sent for tests indicated? x <br /> Were bubbles present in VOA Vials?:(Volatile Methods Only) 7( <br /> Section 3—SummalFtowreu In tor I n fo. <br /> 41aod Summa#: INT A <br /> Unused Summa#: JL N <br /> Cleaning Summa€: <br /> Re ulatorOh <br /> Was there any visual damage to summa c artisters or flow re ulators?E xy IaIn- <br /> Section 4—COC Info. <br /> Com leied into From Completed <br /> Yes N. Comment Yes No Commems <br /> Was COC Received x - Analysis Requested x <br /> Date Sampled x - Samples arrived within holding time x - <br /> Time Sampled x - Any hold times less than 72 hrs. x <br /> Sample fp x - Client Name x - <br /> Rush TAT x -5 day Address/Telephone# x - <br /> Section S—Comments 1 Discrepancies <br /> Was Client notified of discrepancies: NIA Notified by: <br /> Explanations 1 Cotttments: <br /> r <br /> Samples Labeled by: RL Filled out by: Rachele Lang Date:4/8/2019 <br /> BEN: Dept. I 1 Time: 16:59 <br /> CDC ScannedlAttached by: RL <br /> Sample labels reviewed by: RL <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2of2 <br />