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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: [none] Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 02/19/18 19:14 <br /> Total Recoverable Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A\B0183-EPA 7471A <br /> LCS Dup(A\B0183-BSD1) Prepared&Analyzed:02/19/18 <br /> Mercury 0.177 0.016 mg/kg 0.200 88.4 80-120 3.69 20 <br /> Matrix Spike(A\B0183-MS1) Source:1802105-01 Prepared&Analyzed:02/19/18 <br /> Mercury 0.207 0.016 mg/kg 0.200 0.0272 90.0 75-125 <br /> Matrix Spike Dup(A\B0183-MSD1) Source:1802105-01 Prepared&Analyzed:02/19/18 <br /> Mercury 0.214 0.016 mg/kg 0.200 0.0272 93.2 75-125 3.04 20 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 10 of 16 <br />