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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: [none] Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 02/22/18 13:08 <br /> Wet Chemistry-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A\B0198-EPA 9040B <br /> Duplicate(A\B0198-DUPl) Source:1802097-01 Prepared&Analyzed:02/19/18 <br /> pH 12.694 0.10000 pH Units 12.699 0.0394 20 <br /> Duplicate(A\B0198-DUP2) Source:1802125-01 Prepared&Analyzed:02/19/18 <br /> pH 12.643 0.10000 pH Units 12.641 0.0158 20 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 5 of <br />