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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: 2020 Annual Bottom Ash Profiling <br /> 2526 W.Washington St. Project Number: 4700995195 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffman 04/10/20 21:48 <br /> Sample Integrity W0RK ORDER: b <br /> Company Name: <br /> Date Received: 4 ! ! 2C3 New Client: Y <br /> r <br /> tion l —Sample Arrival information <br /> ple Transport: ONTRAC UPS USPS Waik-[n ELCHEIVI Co r Fed-Ex Other: <br /> nsported In: ice Chest ox Hand <br /> Packing materials- Bubble Wrap Foam Packing Peanuts Paper Other: lJ Pe' <br /> Has chilling process begun" Y (,!') Samples Received: Chilled to Touch 1 bi I On Ice <br /> Temperature of Samples("C):_LSL_!�L Ice Chest Temperature(s)(°C)_ <br /> OR"M <br /> —flottle/Analysiis Info. <br /> Yes No NIA Comments <br /> ttles arrive unbroken and intact? <br /> ttle labels agree with COC? <br /> ect containers used for the tests requested? <br /> ct preservations used For the tests requested?cient amount of sample sent for tests indicated?ies present in VOA Vials?:(Volatile Methods Only) <br /> Section 3—Summa/Flow regulator Information ?� <br /> `llaed Suanneci#: <br /> Unused Sumtna#: <br /> Cleaain Summa#: <br /> Ile lator#: <br /> Was there any visual damage to summa canisters or flow regulators?Explain- <br /> Section 4—COC Inroroxation <br /> Yes Nv Comments Yes No Comments <br /> COC Received Analysis Requested <br /> Date Sampled Samples arrived within holding tune <br /> Time Sampled >< Hold times less than 72 hours <br /> Sample ID J Client Name <br /> Rush Turn Around Time 3 bac[ Client Contact Information <br /> SHORT HOLD LLST r7Z hours <br /> H Chlorine Corragivi - Coliform Digsplvcd 4dar Ni[ra[e mm,* Ortho- h�py hate <br /> MBAs .456estos Semple Solids Turbidi Biochemical Dx aemend HPC Color Tediars AmmoniarrKTi un reserved <br /> Section S—Comments I Discre aacies <br /> Client notified ofdiscrepancies; Yes 1 No Notified b <br /> Cowmen <br /> Bin Number/Location: f Filled out by- RD't� l Date; y r-7/2-0COC Sc:nnncdl- ched by; + Time. �❑_S� <br /> Samptes labeled by! <br /> sample labels rcviewrxl by <br /> Excelchem Laboratories.Tnc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2of4 <br />