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Excelchem Laboratories,Inc. <br /> DTE Stockton,LLC Project: 2020 Annual Bottom Ash Profiling <br /> 2526 W.Washington St. Project Number: 4700995195 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffman 04/10/20 21:31 <br /> Sample Lntegrity 'WORK ORDER-e D 01t j w <br /> Company Name: <br /> Date Received. c, I -712b New Client: Y <br /> Section l—Sample Arrival Io formation <br /> Sam pie Transport: ONTRAC UPS USPS Walk-In ELCI iE1Vi Co r Fed-Ex other: <br /> Tmn3ported In: Ice Chest (i h' Hand <br /> Packing materials: Bubble Wrap Foam Packing Peanuts Paper other: V's P— <br /> rias chilling process begun? Y Samples ReceiWed: Chilled to Touch I bin I On Ice <br /> Temperature of Samples(°C). 4 Ice Chest Temperature(s)(°C): _>< <br /> Section 2—BottlafAnalysis Info- <br /> Yes No N/A Comments <br /> Did all bottles arrive unbroken and intact? <br /> Did all bottle labels agree with COC? <br /> Were correct containers used for the tests requested? <br /> Were correct preSeMatiorlS used for the tests requested? <br /> Was a sufficient amount of sample sent for tests indicated? <br /> Were bubbles present in VOA Vials?:(Volatile Methods Oniv) <br /> Section 3—Summa/Flow regulator Information. K� 'b" <br /> `hoed S•" "#-- <br /> Unused Summa#- <br /> Cleaning Sum utaft: <br /> Regulator#- <br /> Was there any visual damage to surnma canisters or flow regulators?Explain. <br /> Section 4—COC Into. <br /> Yes No Comments Yts No Coments <br /> COC Received Analysis Requested m <br /> Date Sampled 1>11 J I I Samples arrived within holding time <br /> Time Sampled >[ Hold tiraes less than'72 hours f <br /> Sample 17D Client Name <br /> Rush Turn Around TimeJ. <br /> 3 DPS{ Client Contact Information <br /> SHORT HIOLD LIST C<72 hours <br /> H Chlorine Corrosivi Coliform Dissolved Odar Nitron. Nitrite orttty- hos hate <br /> MBAs Asbestos Settable Solids Turbidi 13iochemicai Demand I HPC n reserved <br /> Section S—Comments/Discrepancies <br /> Client notified of discrepancies: Yes/No Notified b <br /> Commen - <br /> Sin Number/Location: Filled out by: i � „. Date; y' 71z� <br /> COC ScannedlP.nachrd by t� Time: i0'•Scl <br /> 5arnpies labeled by- <br /> Sample!abets reviewed byr <br /> Excelchem Laboratories.Tnc. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2of4 <br />