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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: #4701180998 Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 06/12/18 17:39 <br /> Total Recoverable Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch AW0058-EPA 7471A <br /> LCS Dup(A\F0058-BSD1) Prepared:06/07/18 Analyzed:06/08/18 <br /> Mercury 0.195 0.016 mg/kg 0.200 97.6 80-120 0.411 20 <br /> Matrix Spike(A\F0058-MS1) Source:1806034-01 Prepared:06/07/18 Analyzed:06/08/18 <br /> Mercury 0.0984 0.016 mg/kg 0.200 0.0936 2.40 75-125 QM-01 <br /> Matrix Spike Dup(A\F0058-MSD1) Source:1806034-01 Prepared:06/07/18 Analyzed:06/08/18 <br /> Mercury 0.170 0.016 mg/kg 0.200 0.0936 38.0 75-125 53.1 20 QM-01 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 8 of 14 <br />