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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: #4701180998 Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 06/13/18 16:19 <br /> Sample Integrity WORK ORDER1804&D5S <br /> V3atc Received:06/07/2018 <br /> Ststi,os l-Sample.�xri,•el Infn_ - <br /> Sas..ple Transpcu�_ f�('E E.t'fiFit7 Courier Ttatl.spured3 tri Mend <br /> fkSLTbI•te lypc of paeltieg nwerial: �Vne <br /> Has chilling ptvacsa begun? NO Samples R id Ai mbieai <br /> Tentperatutr of SanV4cs(`C): ? Ice[`_hexa Te:n +eraturcts]I'Cl: ZYA <br /> Sewn 2--Sutde/Analysis Info- <br /> Va Ph. MA CarrK� <br /> Did all bottles arrire unhrokon and intact? x - <br /> 17id a3F bottle labels agree with CC?C- <br /> Wicre ctvireCl tc+x>Itaincrs used For the te-:Lc ucsted? x - <br /> Wen:conx5c-F atians used fw the Jests rcqwesjcV x <br /> Was a sxlf MCN JAMMnt of samptc sent far Ir$tc iq¢jcyt ? x <br /> Were bubnioS pres.M in VOA Vials?:(VolalDe Methods-Only) x <br /> Secdon 3—SunauralF•low regubatpr info. <br /> - <br /> Unosed 5umnsr*: <br /> Cleauftak tiutnot�d= - <br /> 1ie�talatorih_ -Was there any visual damage to-t nvna can swm or flow rngulator:s'?Rxp6in. <br /> Section d-COC"fo- <br /> CIHT%Idctcd 10h,F snY, C; <br /> Y# N. CYES No C'Llla<aCMS <br /> Was COC Rcceivc d x J - Analysis REquestcd It - <br /> ❑aw Sanded x - samples arrived wilhm boWivs time x - <br /> Time Sailed if Any hc4d bines less Mian 72 itri x <br /> Sample ED x Clienx Nance x <br /> Rush TAT x -2 day Addm&w Tetephone ti x - <br /> Sati4iure 5-Consnteats i Uiscre"ncies <br /> Was Client notit-xtxt 4,1`discrepa les: NQ NFnlified NIA <br /> FXrla alions/Cornmenl-c: <br /> w <br /> —Sw <br /> Labeled b3= JR ruled Out bvt . Date:CvN201.$ <br /> Bm*= tlep[. I 1 TGme: 16:t l <br /> COC Sc-mroedlAltadted by: �H <br /> Sample Labelle reviewed by. JI{ <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2of2 <br />