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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Bottom Ash Truck 1 Q3 Testing <br /> 2526 W.Washington St. Project Number: 4701180998 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 09/17/18 17:09 <br /> STLC Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A\I0069-EPA 7470A <br /> Blank(A\I0069-BLK1) Prepared&Analyzed:09/13/18 <br /> Mercury ND 0.00240 mg/L <br /> LCS(A\I0069-BS1) Prepared&Analyzed:09/13/18 <br /> Mercury 0.0386 0.00240 mg/L 0.0400 96.4 75-120 <br /> LCS Dup(A\10069-BSD1) Prepared&Analyzed:09/13/18 <br /> Mercury 0.0382 0.00240 mg/L 0.0400 95.6 75-120 0.833 20 <br /> Matrix Spike(A\I0069-MS1) Source:1809033-01 Prepared&Analyzed:09/13/18 <br /> Mercury 0.0326 0.00240 mg/L 0.0400 ND 81.6 75-125 <br /> Matrix Spike Dup(A\10069-MSD1) Source:1809033-01 Prepared&Analyzed:09/13/18 <br /> Mercury 0.0325 0.00240 mg/L 0.0400 ND 81.2 75-125 0.491 20 <br /> Batch A\I0086-EPA 6010B <br /> Blank(A\I0086-BLK1) Prepared:09/13/18 Analyzed:09/14/18 <br /> Antimony ND 2.0 mg/L <br /> Arsenic ND 0.2 <br /> Barium ND 0.4 <br /> Beryllium ND 0.1 <br /> Cadmium ND 0.2 <br /> Chromium ND 0.2 <br /> Cobalt ND 1.0 <br /> Copper ND 0.4 <br /> Lead ND 0.2 <br /> Molybdenum ND 0.2 <br /> Nickel ND 0.2 <br /> Selenium ND 0.4 <br /> Silver ND 0.4 <br /> Thallium ND 0.4 <br /> Vanadium ND 0.4 <br /> Zinc ND 0.4 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 12 of 17 <br />