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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Bottom Ash Truck 1 Q3 Testing <br /> 2526 W.Washington St. Project Number: 4701180998 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 09/17/18 19:07 <br /> Total Recoverable Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A\I0091-EPA 7471A <br /> LCS Dup(A\I0091-BSD1) Prepared&Analyzed:09/17/18 <br /> Mercury 0.182 0.016 mg/kg 0.200 90.8 80-120 0.00 20 <br /> Matrix Spike(A\I0091-MS1) Source:1809063-01 Prepared&Analyzed:09/17/18 <br /> Mercury 0.186 0.016 mg/kg 0.200 0.00280 91.4 75-125 <br /> Matrix Spike Dup(A\10091-MSD1) Source:1809063-01 Prepared&Analyzed:09/17/18 <br /> Mercury 0.169 0.016 mg/kg 0.200 0.00280 83.0 75-125 9.48 20 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page II of 17 <br />