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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Bottom Ash Truck 1 Q3 Testing <br /> 2526 W.Washington St. Project Number: 4701180998 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 09/17/18 19:07 <br /> STLC Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A\I0093-EPA 6010B <br /> Matrix Spike(A\I0093-MS1) Source:1809034-05 Prepared&Analyzed:09/17/18 <br /> Antimony 20.1 2.0 mg/L 20.0 0.023 101 75-125 <br /> Arsenic 21.4 0.2 20.0 ND 107 75-125 <br /> Barium 21.4 0.4 20.0 2.13 96.1 75-125 <br /> Beryllium 19.1 0.1 20.0 0.004 95.4 75-125 <br /> Cadmium 20.0 0.2 20.0 0.005 99.8 75-125 <br /> Chromium 19.8 0.2 20.0 0.254 97.5 75-125 <br /> Cobalt 18.9 1.0 20.0 0.337 93.0 75-125 <br /> Copper 19.1 0.4 20.0 0.069 95.1 75-125 <br /> Lead 18.4 0.2 20.0 0.339 90.5 75-125 <br /> Molybdenum 19.7 0.2 20.0 0.048 98.2 75-125 <br /> Nickel 19.7 0.2 20.0 1.15 92.7 75-125 <br /> Selenium 21.3 0.4 20.0 ND 107 75-125 <br /> Silver 19.6 0.4 20.0 ND 98.2 75-125 <br /> Thallium 17.1 0.4 20.0 ND 85.6 75-125 <br /> Vanadium 20.5 0.4 20.0 1.22 96.4 75-125 <br /> Zinc 20.2 0.4 20.0 0.199 100 75-125 <br /> Matrix Spike Dup(A\I0093-MSD1) Source:1809034-05 Prepared&Analyzed:09/17/18 <br /> Antimony 20.4 2.0 mg/L 20.0 0.023 102 75-125 1.18 25 <br /> Arsenic 21.6 0.2 20.0 ND 108 75-125 0.698 25 <br /> Barium 22.2 0.4 20.0 2.13 101 75-125 4.04 25 <br /> Beryllium 19.2 0.1 20.0 0.004 96.2 75-125 0.835 25 <br /> Cadmium 20.2 0.2 20.0 0.005 101 75-125 1.05 25 <br /> Chromium 20.0 0.2 20.0 0.254 98.5 75-125 1.01 25 <br /> Cobalt 19.2 1.0 20.0 0.337 94.1 75-125 1.16 25 <br /> Copper 19.3 0.4 20.0 0.069 96.3 75-125 1.20 25 <br /> Lead 18.6 0.2 20.0 0.339 91.3 75-125 0.864 25 <br /> Molybdenum 19.9 0.2 20.0 0.048 99.2 75-125 1.06 25 <br /> Nickel 19.8 0.2 20.0 1.15 93.5 75-125 0.809 25 <br /> Selenium 21.6 0.4 20.0 ND 108 75-125 1.40 25 <br /> Silver 20.6 0.4 20.0 ND 103 75-125 4.87 25 <br /> Thallium 17.2 0.4 20.0 ND 86.0 75-125 0.525 25 <br /> Vanadium 20.8 0.4 20.0 1.22 98.2 75-125 1.74 25 <br /> Zinc 20.4 0.4 20.0 0.199 101 75-125 1.08 25 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 14 of 17 <br />