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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Bottom Ash Truck 1 Q3 Testing <br /> 2526 W.Washington St. Project Number: 4701180998 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 09/17/18 20:13 <br /> STLC Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A\I0094-EPA 6010B <br /> Matrix Spike(A\I0094-MS1) Source:1809068-02 Prepared&Analyzed:09/17/18 <br /> Antimony 21.4 2.0 mg/L 20.0 0.026 107 75-125 <br /> Arsenic 22.8 0.2 20.0 0.337 112 75-125 <br /> Barium 26.2 0.4 20.0 6.26 99.9 75-125 <br /> Beryllium 19.5 0.1 20.0 0.004 97.4 75-125 <br /> Cadmium 20.9 0.2 20.0 0.016 105 75-125 <br /> Chromium 20.5 0.2 20.0 0.420 100 75-125 <br /> Cobalt 19.2 1.0 20.0 0.117 95.3 75-125 <br /> Copper 21.9 0.4 20.0 2.39 97.7 75-125 <br /> Lead 18.4 0.2 20.0 ND 92.1 75-125 <br /> Molybdenum 20.5 0.2 20.0 0.081 102 75-125 <br /> Nickel 19.6 0.2 20.0 0.710 94.4 75-125 <br /> Selenium 22.3 0.4 20.0 ND 111 75-125 <br /> Silver 19.8 0.4 20.0 ND 98.9 75-125 <br /> Thallium 17.6 0.4 20.0 ND 88.0 75-125 <br /> Vanadium 20.0 0.4 20.0 0.703 96.3 75-125 <br /> Zinc 21.2 0.4 20.0 1.45 98.5 75-125 <br /> Matrix Spike Dup(A\I0094-MSD1) Source:1809068-02 Prepared&Analyzed:09/17/18 <br /> Antimony 20.7 2.0 mg/L 20.0 0.026 103 75-125 3.04 25 <br /> Arsenic 22.3 0.2 20.0 0.337 110 75-125 2.31 25 <br /> Barium 25.8 0.4 20.0 6.26 97.8 75-125 1.61 25 <br /> Beryllium 19.0 0.1 20.0 0.004 94.9 75-125 2.55 25 <br /> Cadmium 20.4 0.2 20.0 0.016 102 75-125 2.51 25 <br /> Chromium 20.0 0.2 20.0 0.420 97.9 75-125 2.42 25 <br /> Cobalt 18.7 1.0 20.0 0.117 92.8 75-125 2.64 25 <br /> Copper 21.6 0.4 20.0 2.39 95.9 75-125 1.61 25 <br /> Lead 18.0 0.2 20.0 ND 89.8 75-125 2.53 25 <br /> Molybdenum 20.0 0.2 20.0 0.081 99.4 75-125 2.67 25 <br /> Nickel 19.1 0.2 20.0 0.710 92.0 75-125 2.43 25 <br /> Selenium 21.8 0.4 20.0 ND 109 75-125 2.27 25 <br /> Silver 19.6 0.4 20.0 ND 98.0 75-125 0.965 25 <br /> Thallium 17.1 0.4 20.0 ND 85.7 75-125 2.71 25 <br /> Vanadium 19.5 0.4 20.0 0.703 93.8 75-125 2.49 25 <br /> Zinc 20.6 0.4 20.0 1.45 95.7 75-125 2.63 25 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 14 of 17 <br />