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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Bottom Ash Truck 1 Q3 Testing <br /> 2526 W.Washington St. Project Number: 4701180998 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 09/18/18 18:12 <br /> Total Recoverable Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A\I0113-EPA 7471A <br /> LCS Dup(A\I0113-BSD1) Prepared&Analyzed:09/18/18 <br /> Mercury 0.193 0.016 mg/kg 0.200 96.4 80-120 3.27 20 <br /> Matrix Spike(A\I0113-MS1) Source:1809083-01 Prepared&Analyzed:09/18/18 <br /> Mercury 0.193 0.016 mg/kg 0.200 0.000880 96.0 75-125 <br /> Matrix Spike Dup(A\10113-MSD1) Source:1809083-01 Prepared&Analyzed:09/18/18 <br /> Mercury 0.199 0.016 mg/kg 0.200 0.000880 99.2 75-125 3.27 20 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 11 of 18 <br />