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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Bottom Ash Truck 1 Q3 Testing <br /> 2526 W.Washington St. Project Number: 4701180998 Date Reported: <br /> Stockton,CA 95203 Project Manager: Genny Huffinan 09/18/18 18:12 <br /> STLC Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A\I0110-EPA 6010B <br /> Matrix Spike Dup(A\I0110-MSD1) Source:1809067-01 Prepared&Analyzed:09/18/18 <br /> Antimony 21.1 2.0 mg/L 20.0 0.094 105 75-125 0.756 25 <br /> Arsenic 22.5 0.2 20.0 0.154 112 75-125 0.400 25 <br /> Barium 19.8 0.4 20.0 0.588 95.8 75-125 1.36 25 <br /> Beryllium 18.6 0.1 20.0 ND 93.2 75-125 0.428 25 <br /> Cadmium 20.7 0.2 20.0 0.009 103 75-125 0.722 25 <br /> Chromium 20.3 0.2 20.0 0.436 99.2 75-125 0.345 25 <br /> Cobalt 18.5 1.0 20.0 0.024 92.2 75-125 0.216 25 <br /> Copper 21.5 0.4 20.0 2.18 96.6 75-125 1.02 25 <br /> Lead 18.2 0.2 20.0 0.014 90.8 75-125 0.0551 25 <br /> Molybdenum 20.5 0.2 20.0 0.344 101 75-125 0.243 25 <br /> Nickel 18.8 0.2 20.0 0.282 92.3 75-125 0.426 25 <br /> Selenium 22.0 0.4 20.0 0.040 110 75-125 0.948 25 <br /> Silver 18.9 0.4 20.0 0.004 94.4 75-125 0.423 25 <br /> Thallium 17.4 0.4 20.0 0.043 86.7 75-125 0.0575 25 <br /> Vanadium 18.7 0.4 20.0 0.446 91.4 75-125 0.804 25 <br /> Zinc 19.6 0.4 20.0 0.050 97.8 75-125 0.102 25 <br /> Batch A\I0114-EPA 7470A <br /> Blank(A\10114-BLK1) Prepared&Analyzed:09/18/18 <br /> Mercury ND 0.000240 mg/L <br /> LCS(A\10114-BS1) Prepared&Analyzed:09/18/18 <br /> Mercury 0.00408 0.000240 mg/L 0.00400 102 75-120 <br /> LCS Dup(A\10114-BSD1) Prepared&Analyzed:09/18/18 <br /> Mercury 0.00389 0.000240 mg/L 0.00400 97.2 75-120 4.82 20 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 14 of 18 <br />