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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: [none] Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 01/11/17 18:46 <br /> DRAFT:Wet Chemistry-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A[A0058-EPA 9040B <br /> Duplicate(A[A0058-DUP1) Source:1701027-02 Prepared:01/06/17 Analyzed:01/11/17 <br /> pH 12.74 0.1000 pH Units 12.77 0.196 20 <br /> Duplicate(A[A0058-DUP2) Source:1701027-02 Prepared:01/09/17 Analyzed:01/11/17 <br /> pH 12.66 0.1000 pH Units 12.77 0.897 20 <br /> Duplicate(A[A0058-DUP3) Source:1701027-02 Prepared:01/10/17 Analyzed:01/11/17 <br /> pH 12.68 0.1000 pH Units 12.77 0.699 20 <br /> Duplicate(A[A0058-DUP4) Source:1701027-02 Prepared&Analyzed:01/11/17 <br /> pH 12.67 0.1000 pH Units 12.77 0.778 20 <br /> DRAFT REPORT The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 18 of 19 <br />