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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: [none] Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 01/25/17 17:05 <br /> Wet Chemistry-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A[A0141-EPA 9040B <br /> Duplicate(A[A0141-DUPl) Source:1701070-01 Prepared&Analyzed:01/16/17 <br /> pH 12.71 0.1000 pH Units 12.69 0.134 20 <br /> Duplicate(A[A0141-DUP2) Source:1701070-01 Prepared&Analyzed:01/17/17 <br /> pH 12.71 0.1000 pH Units 12.69 0.157 20 <br /> Duplicate(A[A0141-DUP3) Source:1701070-01 Prepared&Analyzed:01/18/17 <br /> pH 12.63 0.1000 pH Units 12.69 0.466 20 <br /> Duplicate(A[A0141-DUP4) Source:1701070-01 Prepared&Analyzed:01/20/17 <br /> pH 12.36 0.1000 pH Units 12.69 2.65 20 <br /> Duplicate(A[A0141-DUP5) Source:1701070-01 Prepared&Analyzed:01/23/17 <br /> pH 12.31 0.1000 pH Units 12.69 3.02 20 <br /> Duplicate(A[A0141-DUPE) Source:1701070-01 Prepared&Analyzed:01/24/17 <br /> pH 12.24 0.1000 pH Units 12.69 3.59 20 <br /> EXcelchern Environn-iental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> y custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 8 of <br />