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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: [none] Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 01/25/17 17:05 <br /> Sample Integrity - WORK ORDER : 1701072 <br /> Date Rece jvc:d; /16/2417 <br /> Section 1—Sample Arrival Into. <br /> Sa nple Transporr UPS Transported In! B43X <br /> De�scYibe typi 4of pm kinx rrwtA-6iSlS; Non <br /> Has chilling pro4-e.se trcgwn,° Iso 's;1313ryle14 Re!CUiuptl; AmW4!n! <br /> Tcfnpersturi-,of Swnples{gC); Ifi Ice ChcsE Tcntiperaturc(s) <br /> Section 2—HattliYAnalysks Infu. <br /> Did a]1 bacrl s arrive uiibrokeo:nO inta4t'21 x - <br /> Did'a31 hnule laloeLti i4g7r=with COC? x - <br /> Were cQrr i;1 comminors used for the testa r ucsted? x <br /> Wr-rc correct pireservations used for the nests requested? X - <br /> Was a sufficieru amoum or sample 46nit tore tr iudicatcd7 x - <br /> VYere bubbles present in VOA ViaW.-.(Volatile Methods[.1rxly) x - <br /> Section 3 — SuirnrnalF.Jow regulator Info- <br /> Uirudued t3ummaC <br /> fi)leanIOU.}u.nlm0N: <br /> Rcxpiator#; <br /> Was there any vixu;d damn to summa canisters or flaw r1R;gul3tn3s4 7'XP[uin. <br /> Section 4—COU Into. <br /> {%anPlcta] fnfo Prawn <br /> .. <br /> Yrs Na Q. r+Lg YON No Carrtrnents <br /> Was COC Received x Anaiysin R uexted x - <br /> Date Sampled 1( Samples urrived within hnidrng rJme x _ <br /> 74mc Sampled x Any hold times less ehan 72 hrs x <br /> Sample ID x - Client Nan-Le x <br /> Rush <br /> TAT <br /> X AddresslTelcphot5e# <br /> Section 5—Caaniner is/Disc rCRll ncies <br /> Was Clioni nofifled of discre anrriv-v; NIA Noflfled by: NIA <br /> Ex ]ar,;�#ions!Canunenls: - .. <br /> S w Lrti LabrlerJ hy_ ,JL Filled L i DWe= 11I()f17 <br /> Bio = DEPT.]i h[ <br /> yTime: l 1-52 <br /> OW Scanntdlhsraahed by- JL <br /> S>1tt le labe3s reviewt5d <br /> ay' - <br /> EXcelchern Envlronn-iental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> y custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2of2 <br />