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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: [none] Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 02/07/17 15:07 <br /> Wet Chemistry-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A[A0146-EPA 9040B <br /> Duplicate(A[A0146-DUPl) Source:1701107-01 Prepared&Analyzed:01/24/17 <br /> pH 13.20 0.1000 pH Units 12.92 2.14 20 <br /> Duplicate(A[A0146-DUP2) Source:1701107-01 Prepared&Analyzed:01/25/17 <br /> pH 13.17 0.1000 pH Units 12.92 1.94 20 <br /> EXcelchern Environn-iental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> y custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 6 of <br />