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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: [none] Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 02/08/17 17:54 <br /> Sarnple Integrity WORK ORDER : 1702002. <br /> Date Received: 02/01!2017 <br /> SLCtiot! 1 — Aatple Arrives] Enru.- <br /> !:,rnply Transport; EXCEJ AHEM Courier Transported In-, H,_nd <br /> Describe type of packing materials: None <br /> Has chilling process begun? No Samples Recaiwcd; _ nibieng <br /> Temperature of Samples ( C): 16 Icc Chest Ternpel'atxlre{s) (¢C);1sUA <br /> Rection 2—KottlaAoulyxis Ingo. <br /> Yaa Ko Kfk Comuwr s <br /> Did all bottles arrivc unbroken and intact? x <br /> Did all battle labels agree with COC"? x <br /> Were correct cotrtainers used for rhe textX ne raV-,Jt5 P' x - <br /> ere CL3rrt1AA i�--serv;tlions used for the tests requested? x - <br /> W;ss x sufticicnt ttrrtount ofsam le sent for tests indicated? ] <br /> were bubbEca presenr in VOA VkLLs?=(Yolalile Method .Only] x <br /> Section 3 —Surnma Flc w rc ulator Info. <br /> Unused wiutllMSOL <br /> UlEaIJUK SumnvtN: <br /> EReRu]atprAFe ..._ <br /> Wm ihei%a airy visual dairtage to smrnma canisters or Flow regulators?Explain. <br /> Section 4—COC lnCo. <br /> Cam Ined Tnf.Fnin C Iat�vJ <br /> Yvx .�"u C+o.}w:nc Ycyc Nrr C'�rrynprC6 <br /> Was U-10C Retxrwed x Analysis Requested x <br /> Date Sampled x Smrlpl"arrivrd within holding Limo x <br /> Time Sampled x Auy hoI J times less than 72 hra x <br /> Sample ID x Client Numc x <br /> lZush TAT x AOdressrreie ane# x <br /> Section 5—Comments}Dis�crepaneieg <br /> Wfls Ciicrtl norificd of discre aOCi St NIA NatiFed by: NIA <br /> fisc 1�1n:11iVri�f CVminenlS: -' ----- <br /> `3amglez LahtLed bY= JL. Filled t7&.'e "' I?8te: 2}1}17 <br /> Bin#S: I?>EF'T,11 �[ Time: 12:22 <br /> COC 3cann,,vl;ucche—by_ JL <br /> Sample Label%reviewed <br /> by: <br /> Excelchern Environn-iental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2of2 <br />