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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: [none] Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 03/21/17 13:41 <br /> Sample Integrity WORK ORDER = 1703044 <br /> Date Receivod: 03/07/2017 <br /> Section i —Sample Arrival ]or'V, <br /> ;3r�5111e rr.angp+l[#: ECE-LCHEM Courirr Tr.lnxportad ln. IKC Gudest <br /> l-3v*1;ribs typo of packing materials: Nvnc <br /> Has chilling process begun? Yes Samples Received, Ambient <br /> Temperature of samples('C): ZLI ice Chet Tarrlperaturm(s) (OC)na <br /> geCtion 2—130tilt)Aonlyuis Info. - <br /> _ Yeo- No N1.4 Cankmrrrs <br /> Dice;All wntainm-s arrive unbroken and inmcO x - <br /> Did all container l abels agree with COC? x <br /> Were cormm comaiucrs used Fnr the to'Su;r ucsWCY,' x <br /> Were correct prewer atiQns used for the tests r uested? x <br /> Wac A svffiticnt amount of sam lc sent for tests indicated'? x - <br /> t1 CM bubbleS petse[«in VOA Vials?:(Volntile Meth 4r'Only) x _ <br /> Section :t — SL1Ynl: a/F[gvw rc ulator Info. <br /> Meed Sunt masse <br /> Umvrcd Summa*: X11 A <br /> Cleaatiid t3ummaM: <br /> Re ulatorN! <br /> Was rhtxe any visual darr,a a try summa canisters or flow regulators?Explain. <br /> Soetion 4—COC Info. <br /> Com le�etl TnfaARam C leted <br /> Yas N4 ONAL.L.— YCo- }"1a C'ammenis <br /> wgkw COC Received x - Aualy tk Reque$LtZ�¢ x - <br /> Vate Sampled x Sanwh3s arrived within holding lime x <br /> Time Sampled x Arly hold times less than 72 hrs x <br /> Samplc ID x Client Mame x <br /> Rush TAT x Addressirelephcne# x <br /> SCCLIon S—CtmsmeuIN f DlscrepanCivs <br /> Was CECTtc noTiFed of discrepancies: NfA _ Notified by: NIA <br /> 1=x lan�ti�,ns I Comments; - . <br /> Samples Labeled by: ,J',j Filled r te, Dmie: 317!17 <br /> - out <br /> Bin*%: 17¢�1L 11 hy., lri—cq 14;QU <br /> t+7C scmorS+Anrc�oct hy: JS <br /> Sample latclx rpvicwad <br /> by: <br /> Excelchem.Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2of2 <br />