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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: 4701052861 Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 08/10/17 17:15 <br /> Sample Integrity WORK ORDUR ; 1705050 <br /> Date Received= Q3YD2J2p17 <br /> $ectiun I—Sample Arrival Info. <br /> Sample Transpon-. FiXCELCHJEM Courier Tranxporuad Irl; lee Cheat <br /> Describes type c f packing materials! Nage <br /> Has chilling process begun? Yes Siimples Received; -._.Qu ICE <br /> TernperaLurc of samples(4C}: 21 [ce wheat Temperatu�e(s) CSC}?e4 <br /> Bectiun 2—SoltlelAnalysis Info. <br /> Yaa tfo NIA Cam herhu <br /> Did Intl containers arrive unbroken and inraor'} x - <br /> Did all oontainer labels agree with COC---) x <br /> Were eorrecrcontulrwrAE used for Rhe tests uested7 x - - <br /> Wcre corrnGt prcscrvatians used far the tester ucsted? x <br /> Was a sufficient amount of satn to sant for tesrs lndlcared7 x <br /> Were bubblers present in VOA Vial$?;(Volatllc mcctwtis Only) x <br /> Section 3 —SummalFlow re ulator Info. <br /> Unused Summnlie <br /> Clrnning Summa#: <br /> RegalatorM <br /> Wn,5 there any visual damage to sump-La canisrem l►r Clow reaulacprL3'!U0Xp&i,w- <br /> Settian 4—COC Cnfp. <br /> Com Iclod Info Fraun l: lerol <br /> Yes No C.muminer Yes T,o Commen�x <br /> Was COC P'-ceived x - Analysis uestcd <br /> Dale Sampled x - Snnples orr1vap wiihln holding Ilett <br /> -rime yarn lad x An hold times less than 72 hrs x <br /> Sample ID x Clleni Name x <br /> Rush TAT x 7-day Addresfi Telcphonc# x <br /> TAT <br /> Section 5—Comments f Discrepancies— <br /> Was Clierr4 ndmifiad of discrepancies; NIA Nodfied by-- NJA <br /> Ex lanations l Cornmenis-, <br /> Snmplor Labeled by_ JH F111vd r xxa u�a ta+ Dn#e; gni[7 <br /> _ rn�t <br /> Hinat- iii by, Tirne:$:15 <br /> coc sc.wuugAi,cued by; JH <br /> ,;arnplc Ipbels rowicwed JH <br /> by: <br /> Excelchern Envlronn-iental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 2of2 <br />