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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: [none] Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 11/20/17 08:53 <br /> Sample Integrity WORK ORDER : 1709102 <br /> Date Received:09/13/2017 <br /> Section 1--Sample Arrival Info. <br /> Sample Transport: EXCEL CHEM Courier Transported In: BOX <br /> Describe type or packing materials: None <br /> Has chilling process begun? No Samples Recwived: Ambient <br /> Temperature of Sampics(,c): 21 Ice Chest Temperatures)(`C): L7 <br /> Section 2—Bottle/Analysis Info. <br /> Yes No WA C:omrtrnla <br /> Did all bottles arrive unbroken and intact? x - <br /> Did all bottle labels agree with COC? x <br /> Were correct containers used for the tests requested? x <br /> Were correct preservations used for the tests requested? x <br /> Was a sufficient amount of sample sent for tests indicated? x <br /> Were bubbles present in VOA Vials?:(Volatile Methods Only) X <br /> Section 3--Sumtntf/Flow mgulntor Info. <br /> `Flood Sunr�na#: <br /> Unused Sum ma#: <br /> Cleanin summati; <br /> Regulator#. <br /> Was there any visual damage to summa can eters or flow regulators?Explain. <br /> Section 4—COC Info. <br /> ConVlemd Info From Com acted <br /> Yeas No Cc�nt Yes No Comments <br /> Was COC Received x - Analysis Requested x - <br /> Date Sam led x - Samples arrived wishin holding time x <br /> Time Samplcd x - Any hold times less than 72 hrs x <br /> Sample ID x - Client Name x _ <br /> Rush TAT x Address/Telephone# x - <br /> Section 5—Comments I Discrepancies <br /> Was Client notified of discrepancies: NIA ' Notified by* NIA <br /> Explanations/Comments: - <br /> samples Labeled by= AT Pilled out by: 74V(0% Date:9/18/2017 <br /> Sin#s: Dept 1 l Time: 13:20 <br /> COC Scanned/Attached by: AT <br /> Sample labels reviewed by: AT <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative rage 1 oft <br />