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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: 4701052861 Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 11/10/17 17:33 <br /> Wet Chemistry-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A[K0074-EPA 9040B <br /> Duplicate(A[K0074-DUPl) Source:1711039-01 Prepared&Analyzed: 11/09/17 <br /> pH 11.790 0.10000 pH Units 11.759 0.263 20 <br /> Duplicate(A[K0074-DUP2) Source:1711054-01 Prepared&Analyzed: 11/09/17 <br /> pH 12.024 0.10000 pH Units 12.040 0.133 20 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 6 of 16 <br />