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Excelchem Environmental Labs <br /> DTE Stockton,LLC Project: Ash <br /> 2526 W.Washington St. Project Number: 4701052861 Date Reported: <br /> Stockton,CA 95203 Project Manager: Dan Crawford 11/10/17 17:33 <br /> Total Recoverable Metals-Quality Control <br /> Reporting Spike Source %REC RPD <br /> Analyte Result Limit Units Level Result %REC Limits RPD Limit Notes <br /> Batch A[K0064-EPA 7471A <br /> LCS Dup(A[K0064-BSD1) Prepared&Analyzed: 11/09/17 <br /> Mercury 0.188 0.016 mg/kg 0.200 94.0 80-120 0.426 20 <br /> Matrix Spike(A[K0064-MS1) Source:1711033-01 Prepared&Analyzed: 11/09/17 <br /> Mercury 0.255 0.016 mg/kg 0.200 0.0701 92.6 75-125 <br /> Matrix Spike Dup(A[K0064-MSD1) Source:1711033-01 Prepared&Analyzed: 11/09/17 <br /> Mercury 0.248 0.016 mg/kg 0.200 0.0701 89.0 75-125 2.86 20 <br /> Excelchem Environmental Lab. The results in this report apply to the samples analyzed in accordance with the chain of <br /> custody document.This analytical report must be reproduced in its entirety. <br /> Laboratory Representative Page 10 of 16 <br />