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l 1534 Willow Pass Road,Pittsburg,CA 94565-1701 M c C a m p b e I l Analytic al, Inc. Toll Free Telephone:(877)252-9262/Fax:(925)252-9269 "When Quality Countsrr http://www.mccanTbell.com/E-mail:main@mccmVbell.com Quality Control Report Client: GHD Services,Inc. WorkOrder: 1910581 Date Prepared: 10/11/19 BatchID: 186992 Date Analyzed: 10/15/19 Extraction Method: SW5030B Instrument: GC16 Analytical Method: SW8260B Matrix: Soil Unit: mg/kg Project: 11202858-07.11;Chevron 372736-UDC Removal Sample ID: MB/LCS/LCSD-186992 1910581-003AMS/MSD QC Summary Report for SW8260B Analyte LCS LCSD SPK LCS LCSD LCS/LCSD RPD RPD Result Result Val %REC %REC Limits Limit Acetone 0.22 0.22 0.20 112 108 59-127 4.13 20 tert-Amyl methyl ether(TAME) 0.016 0.015 0.020 78 75 54-98 3.09 20 Benzene 0.018 0.017 0.020 90 87 71-115 3.50 20 Bromobenzene 0.017 0.016 0.020 86 81 69-120 6.16 20 Bromochloromethane 0.016 0.016 0.020 81 78 63-117 3.98 20 Bromodichloromethane 0.015 0.015 0.020 77 75 61-109 2.75 20 Bromoform 0.011 0.010 0.020 53 52 46-87 1.68 20 Bromomethane 0.018 0.017 0.020 93 87 22-195 6.01 20 2-Butanone(MEK) 0.071 0.073 0.080 89 91 53-124 2.33 20 t-Butyl alcohol(TBA) 0.067 0.059 0.080 84 73 29-142 13.3 20 n-Butyl benzene 0.032 0.031 0.020 158 156 102-169 0.913 20 sec-Butyl benzene 0.028 0.027 0.020 140 137 100-166 2.61 20 tert-Butyl benzene 0.021 0.022 0.020 107 108 91-153 0.558 20 Carbon Disulfide 0.018 0.018 0.020 91 88 60-125 3.90 20 Carbon Tetrachloride 0.017 0.017 0.020 85 83 69-124 2.91 20 Chlorobenzene 0.017 0.016 0.020 83 82 73-116 1.11 20 Chloroethane 0.020 0.018 0.020 98 92 47-140 5.45 20 Chloroform 0.018 0.017 0.020 89 86 69-118 3.37 20 Chloromethane 0.020 0.019 0.020 101 95 30-132 5.95 20 2-Chlorotoluene 0.021 0.020 0.020 104 101 75-147 2.88 20 4-Chlorotoluene 0.020 0.020 0.020 102 99 75-137 2.16 20 Dibromochloromethane 0.015 0.014 0.020 73 71 57-105 2.60 20 1,2-Dibromo-3-chloropropane 0.0073 0.0070 0.010 73 70 36-103 3.59 20 1,2-Dibromoethane(EDB) 0.0081 0.0080 0.010 81 80 66-101 2.01 20 Dibromomethane 0.015 0.015 0.020 75 73 61-103 1.76 20 1,2-Dichlorobenzene 0.015 0.015 0.020 76 75 59-104 1.93 20 1,3-Dichlorobenzene 0.019 0.018 0.020 93 92 70-133 1.82 20 1,4-Dichlorobenzene 0.017 0.017 0.020 87 85 68-123 2.51 20 Dichlorodifluoromethane 0.0090 0.0081 0.020 45 41 13-107 9.93 20 1,1-Dichloroethane 0.018 0.018 0.020 91 88 69-118 3.68 20 1,2-Dichloroethane(1,2-DCA) 0.018 0.017 0.020 89 86 59-112 3.28 20 1,1-Dichloroethene 0.018 0.017 0.020 89 86 69-126 4.34 20 cis-1,2-Dichloroethene 0.017 0.017 0.020 85 83 69-116 2.95 20 trans-1,2-Dichloroethene 0.017 0.016 0.020 83 80 73-116 3.61 20 1,2-Dichloropropane 0.017 0.016 0.020 83 81 65-111 3.03 20 1,3-Dichloropropane 0.017 0.017 0.020 87 85 67-110 1.83 20 2,2-Dichloropropane 0.020 0.019 0.020 100 97 65-125 3.23 20 1,1-Dichloropropene 0.018 0.018 0.020 91 88 70-123 3.42 20 (Cont.) CA ELAP 1644•NELAP 4033ORELAP Page 54 of 72