Laserfiche WebLink
i <br /> CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive, Atwater, CA 95301 Phone: (209) 384-2930 <br /> Certificate #2480 Fax: (209) 384-1507 <br /> Technicon Engineering Client Project ID: 180321 Method: EPA 5030/8260B <br /> 4539 N. Brawley #108 Lab Reference Number: 1805035 Instrument ID: VARIAN MS <br /> Fresno, CA 93722 Sample Description: Soil Prepared: 05-15-18 <br /> Attn: Steve Curra Analyzed: 05-15-18 <br /> Reported: 05-16-18 <br /> QUALITY CONTROL DATA REPORT <br /> SPIKE ID: VSMS-5158 DP <br /> Reporting BLANK Spiking Control %R <br /> Limit Result Level Spike Limits <br /> mg/Kgmg/Kgmg/Kg %R <br /> COMPOUNDS <br /> t-Bu ( Alcohol t-BA 0.10 NO 3.0 82.0% 70-130 <br /> Meth I t-bu I ether MTBE 0.0050 ND 0.10 92.0% 70-130 <br /> Diiso ro lather DIVE 0.0050 ND 0.10 99.2% 70-130 <br /> Ethyl[ t-Bu I ether ETRE 0.0050 NO 0. 10 93.2% 70-130 <br /> t-Ammeth ether AME 0.0050 NO 0. 10 96.4% 70-130 <br /> Dichloroethane 1 ,2-13CA 0.0050 NO 0. 10 94.4% 70-130 <br /> Eth lane dibromide EDB 0.0050 NO 0.1095.6% 70-130 <br /> 1 , 1 -Dichloroethene 111 ,DCE 0.0050 NO 0.10 91 .6% 70-130 <br /> Benzene 0.0050 ND 0.10 89.6% 70-130 <br /> Trichloroethene (TCE) 0.0050 NO 0.10 96.0% 70-130 <br /> Toluene 0.0050 ND 0. 10 116% 70-130 <br /> Chlorobenzene 0.0050 NO 0.10 1010/0 70-130 <br /> Surro ate: <br /> Dibromofluoromethane 0. 10 104% 0.40 100% 70-130 <br /> 1 ,2-Dichloroethane-d4 0. 10 99.6% 0.40 95.2% 70-130 <br /> Toluene-d8 0.10 93.9% 0.40 103% 70-130 <br /> 4-Bromofluorobenzene 0.10 119% 0.40 108% 70-130 <br /> Spiking MATRIX MATRIX %R %RPD <br /> Level SPIKE SPIKE DUP Limits <br /> mg/Kg %R %R <br /> COMPOUNDS <br /> t-But ill Alcohol (t-13A) 3.0 95.6% 110% 60-130% 13.6% <br /> Meth I t-but I ether MTBE 0.10 92.4% 102% 70-130% 9.33% <br /> Diiso ro I ether DIPE 0.10 99.6% 100% 70-130% 2.37% <br /> Eth I t-But I at ETBE 0. 10 84.0% 876% 70-130% 3.74% <br /> t-Am I meth I ether TAME 0.10 98.0% 100% 70-130% 2.40% <br /> 1 ,2-Dichloroethane 1 12-L)UAI 0.10 95.6% 100% P70-130% <br /> 30% 4.72% <br /> Ethylene dibromide EDB 0. 10 86.8% 97.6% 11 .6% <br /> 1 ,1 -Dichloroethene 1 ,1 ,DCE 010 87.2% 920% 30/ 5.22% <br /> Benzene 0.10 89.6% 94.4% 30% 5.11Trichloroethene TCE 0. 10 118% 127% 30% 7.38% <br /> Toluene 0.10 98.8% 102% 130% 3,55% <br /> Chlarobenzene010 920% 96.4% 130% 4.59% <br /> Surrogate: <br /> Dibromofluoromethane 0.40 99.5% 98.2% D <br /> 1 ,2-Dichloroethane-d4 0.40 103% 105% <br /> Toluene-d8 0.40 96J % 101 % 1 170A o <br /> 4-Bromofluorobenzene 0.40 1 6% 113% 1 70-130% <br /> JUN 2. 5 2018 <br /> APPROVED BY: <br /> James C. Phillips / a oratory Directoro,C <br /> ClariJ. Cone / Lab ratory /Wanager tNVIRONMENTAL HEALTH <br /> DEPARTMENT <br />