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CASTLE ANALYTICAL LABORATORY <br /> Environmental Testing Services 2333 Shuttle Drive, Atwater, CA 95301 Phone: (209) 384-2930 <br /> Certificate #2480 Fax: (209) 384-1507 <br /> Technicon Engineering Client Project Name: 180321 Sampled: 10-04-19 <br /> 4539 N. Brawley #108 Lab Reference Number: 1910022 Received: 10-07-19 <br /> Fresno, CA 93722 Sample Description: Soil Extracted: 10-10-19 <br /> Attn: Steve Curra Sample Prep/Analysis Method: EPA 5030/8260B Analyzed: 10-10-19 <br /> Lab Numbers: 1910022 . 03 Reported: 10-16-19 <br /> Sample ID: S2 @ 9' <br /> VOLATILE ORGANICS - EPA METHOD 8260 GCiMS <br /> REPORTING POL SAMPLE REPORTING PQL SAMPLE <br /> ANALYTE LIMIT RESULT ANALYTE LIMIT RESULT <br /> m Ik m m Ik (mg/kg) (mg/kg) m /k <br /> Acetone 0.050 0.050 NO cis-1 3-Dichloro ro ene 0.0050 0.0050 ND <br /> Benzene 0.0050 0.0050 ND trans-1 3-Dichloro ro ene 0.0050 0.0050 ND <br /> Bromobenzene 0.0050 0.0050 ND Eth (benzene 0.0050 0.0050 ND <br /> Bromochloromethane 0.0050 0.0050 ND Hexachlorobutadiene 0A050 0.0050 ND <br /> Bromodichloromethane 0.0050 0.0050 NO 2-Hexanone 0.050 0.050 NO <br /> Bromoform 0.0050 0.0050 ND Iso ro (benzene 0.0050 0.0050 NO <br /> Bromomethane 0.0050 0.0050 ND -Iso ro (toluene 0.0050 0.0050 ND <br /> n-Butylbenzene 0.0050 0.0050 ND Methylene chloride 0.0050 0.0050 ND <br /> sec-Bu (benzene 0.0050 0.0050 NO Meth Ethyl Ketone MEK 0.050 0.050 ND <br /> tart-Bu (benzene 0.0050 0.0050 NO Methyl isobu I ketone MIBK 0.050 0.050 ND <br /> Carbon tetrachloride 0.0050 0.0050 NO Na thalene 0.0050 0.0050 ND <br /> Chlorobenzene 0.0050 0.0050 ND n-Propylbenzene 0.0050 0.0050 ND <br /> Chlorodibromomethane 0.0050 0.0050 ND Styrene 0.0050 0.0050 ND <br /> Chloroethane 0.0050 0.0050 ND 11 ,1 ,2-Tetrachloroethane 0.0050 0.0050 ND <br /> Chloroform 0.0050 0.0050 NO 11 ,22,-Tetrachlorethane 0.0050 0.0050 NO <br /> Chloromethane 0.0050 0.0050 NO Tetrachloroethene PCE 0.0050 0.0050 ND <br /> 2-chlorotoluene 0.0050 0.0050 ND Toluene 0.0050 0.0050 <br /> NO <br /> 4-Chlorotoluene 0.0050 0.0050 ND 1 ,2 3-Trichlorobenzene 0.0050 0.0050 <br /> 1 ,2-Dlbromo-3-chloro ro ane 0.0050 0.0050 ND 124-Trichlorobenzene 0.0050 0.0050 <br /> 12-Dibromoethane EDB 0.0050 0.0050 ND 11 ,1-Trichloroethane 0.0050 0.0050 <br /> Dibromomethane 0.0050 0.0050 NO 1 , 12-Trichloroethane 0.0050 0.0050 <br /> 1 ,2-Dichlorobenzene 0.0050 0.0050 ND Trichloroethene TCE 0.0050 0.00501 ,3-Dichlorobenzene 0.0050 0.0050 NO Trichlorofluoromethane 0.0050 0.00501 ,4-Dichlorobenzene 0.0050 0.0050 ND 1 2 3-Trichloro ro ane 0.0050 0.0050Dichlorodifluoromethane 0.0050 0.0050 ND 1 ,24-Trimeth (benzene 0.0050 0.0050 <br /> 1 ,1 -Dichloroethane 0.0050 0,00601 ND 1 ,3,5-Trimeth Ibenzene 0.0050 0.0050 1 ND <br /> 1 ,2-Dichloroethane 1 ,2-DCA 0.0050 0.0050 NO Vinyl Chloride 0.0050 0.0050 ND <br /> 1 ,1 -Dichloroethene 0.0050 0.0050 NO Xylenes, total 0.0050 0.0050 NO <br /> cis-12-Dichloroethene 0.0050 0.0050 NO Oxygenates <br /> 0.0050 0. <br /> trans-1 ,2-Dichloroethene 0050 NO tert-ButylAlcohol tBA 0.050 0.050 ND <br /> 1 ,2-Dichloro ro ane 0.0050 0.0050 ND Methyl tert-Butyl Ether MTBE 0.0050 0.0050 NO <br /> 1 ,3-Dichloro ro ane 0.0050 0.0050 ND Di•Iso ro I Ether DIPE 0.0050 0.0050 ND <br /> 2,2-Dichloro ro ane 0.0050 0.0050 ND Eth I tert-But I Ether EtBE 0.0050 0.0050 NO <br /> 1 ,1-Dichloro ro ene 0.0050 0.0050 ND tert-Am I Methy Ether tAME 0.0050 0.0050 ND <br /> Surrogate Recoveries <br /> Dibromofluoromethane 86.6% Toluene-d8 94.0% <br /> 1 ,2-Dichloroethane-d4 77.4% p-Bromofluorobenzene 115% <br /> Instrument ID: VARIAN MS <br /> Analytes reported as ND were not detected or below the Practical Quantitation Limit. <br /> Practical Quantitation Limit (PQL) = Reporting Limit x Dilution Factor <br /> (mg/kg) = milligrams per kilogram or parts per million (ppm) <br /> APPROVED BY: <br /> ClariJ. Cone / Laboratory irector <br /> Cassandra J.A. Nanny/ hemist <br />